7-benzylidene-2,2-dimethyl-3,3a,4,5,6,7-hexahydro-2H-indol-3a-yl benzoate

Base Information

Chemical Name:7-benzylidene-2,2-dimethyl-3,3a,4,5,6,7-hexahydro-2H-indol-3a-yl benzoate
CAS No.:90595-96-3
Molecular Formula:C₂₄H₂₅NO₂
Molecular Weight:359.468
Hs Code.:

Synonyms:7-benzylidene-2,2-dimethyl-3,3a,4,5,6,7-hexahydro-2H-indol-3a-yl benzoate

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Chemical Property of 7-benzylidene-2,2-dimethyl-3,3a,4,5,6,7-hexahydro-2H-indol-3a-yl benzoate

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Technology Process of 7-benzylidene-2,2-dimethyl-3,3a,4,5,6,7-hexahydro-2H-indol-3a-yl benzoate

There total 4 articles about 7-benzylidene-2,2-dimethyl-3,3a,4,5,6,7-hexahydro-2H-indol-3a-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 98-88-4
benzoyl chloride

: 89718-66-1
7-benzylidene-2,2-dimethyl-3,3a,4,5,6,7-hexahydro-2H-indole 1-oxide

: 90595-96-3
7-benzylidene-2,2-dimethyl-3,3a,4,5,6,7-hexahydro-2H-indol-3a-yl benzoate

Guidance literature:: In diethyl ether; Ambient temperature;

Reference yield:

: 78354-75-3
2-(2-Methyl-2-nitro-propyl)-6-[1-phenyl-meth-(E)-ylidene]-cyclohexanone

: 90595-96-3
Benzoic acid 2,2-dimethyl-7-[1-phenyl-meth-(E)-ylidene]-2,3,4,5,6,7-hexahydro-indol-3a-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Zn, NH₄Cl / tetrahydrofuran; H₂O / 3 h / 0 °C

2: diethyl ether / 1 h / Ambient temperature

With ammonium chloride; zinc; In tetrahydrofuran; diethyl ether; water;

Reference yield:

: 5682-83-7
2-Benzylidenecyclohexanone

: 90595-96-3
Benzoic acid 2,2-dimethyl-7-[1-phenyl-meth-(E)-ylidene]-2,3,4,5,6,7-hexahydro-indol-3a-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Me₂NH*HCl; 2) NaOH / 1) EtOH, reflux; 2) reflux, 4 h

2: Zn, NH₄Cl / tetrahydrofuran; H₂O / 3 h / 0 °C

3: diethyl ether / 1 h / Ambient temperature

With sodium hydroxide; N,N-dimethylammonium chloride; ammonium chloride; zinc; In tetrahydrofuran; diethyl ether; water;