tetra-n-butylammonium salt of (p-nitrophenyl)malononitrile

Base Information

• Chemical Name: tetra-n-butylammonium salt of (p-nitrophenyl)malononitrile
• CAS No.: 91879-97-9
• Molecular Formula: C₉H₄N₃O₂*C₁₆H₃₆N
• Molecular Weight: 428.618
• Mol file: 91879-97-9.mol

Synonyms:tetra-n-butylammonium salt of (p-nitrophenyl)malononitrile

Chemical Property of tetra-n-butylammonium salt of (p-nitrophenyl)malononitrile

Chemical Property:

Purity/Quality:

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Technology Process of tetra-n-butylammonium salt of (p-nitrophenyl)malononitrile

There total 2 articles about tetra-n-butylammonium salt of (p-nitrophenyl)malononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Nitrophenylacetonitrile (555-21-5,34512-13-5,174848-08-9) → tetra-n-butylammonium salt of (p-nitrophenyl)malononitrile (91879-97-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran

2: H₂O; ethanol / 50 °C

With sodium hydride; In tetrahydrofuran; ethanol; water;

DOI:10.1021/ja00334a043

Reference yield:

2-(4-nitrophenyl)malononitrile (7077-65-8) + tetra(n-butyl)ammonium hydroxide (2052-49-5) → tetra-n-butylammonium salt of (p-nitrophenyl)malononitrile (91879-97-9)

Guidance literature:

In ethanol; water; at 50 ℃;

DOI:10.1021/ja00334a043

upstream raw materials:

2-(4-nitrophenyl)malononitrile

tetra(n-butyl)ammonium hydroxide

4-Nitrophenylacetonitrile