4-thioformylmorpholine

Base Information

Chemical Name:4-thioformylmorpholine
CAS No.:5780-30-3
Molecular Formula:C₅H₉NOS
Molecular Weight:131.199
Hs Code.:

Synonyms:4-thioformylmorpholine

Suppliers and Price of 4-thioformylmorpholine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-thioformylmorpholine

Chemical Property:

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Technology Process of 4-thioformylmorpholine

There total 3 articles about 4-thioformylmorpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 110-91-8,99108-56-2
morpholine

: 2944-05-0,767590-23-8
carbon monosulfide

: 5780-30-3
4-thioformylmorpholine

Guidance literature:: In toluene; at -78 ℃; under 0.05 Torr;
DOI:10.1021/jo00382a038

Reference yield:

: 110-91-8,99108-56-2
morpholine

: 877465-02-6
dithioformic acid 4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester

: 5780-30-3
4-thioformylmorpholine

: 177971-45-8
4-t-butyl-2,6-bis[(2,2,6,6-tetramethyl-m-terphenyl-2'-yl)methyl]benzenethiol

Guidance literature:: dithioformic acid 4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester; With 2,2,6,6-tetramethylpiperidinyl-lithium; In tetrahydrofuran; at -78 ℃; for 1h;

morpholine; In tetrahydrofuran; at -78 - -30 ℃;
DOI:10.1246/cl.2005.1674