(Z)-1-(3-(2-isopropylphenyl)-4-oxothiazolidin-2-ylidene)-3-(4-(5-(4-(perfluoroethoxy)phenyl)-1,3,4-oxadiazol-2-yl)phenyl)urea

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Chemical Name:(Z)-1-(3-(2-isopropylphenyl)-4-oxothiazolidin-2-ylidene)-3-(4-(5-(4-(perfluoroethoxy)phenyl)-1,3,4-oxadiazol-2-yl)phenyl)urea
CAS No.:1417885-24-5
Molecular Formula:C₂₉H₂₂F₅N₅O₄S
Molecular Weight:631.583
Hs Code.:

Synonyms:(Z)-1-(3-(2-isopropylphenyl)-4-oxothiazolidin-2-ylidene)-3-(4-(5-(4-(perfluoroethoxy)phenyl)-1,3,4-oxadiazol-2-yl)phenyl)urea

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Chemical Property of (Z)-1-(3-(2-isopropylphenyl)-4-oxothiazolidin-2-ylidene)-3-(4-(5-(4-(perfluoroethoxy)phenyl)-1,3,4-oxadiazol-2-yl)phenyl)urea

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Technology Process of (Z)-1-(3-(2-isopropylphenyl)-4-oxothiazolidin-2-ylidene)-3-(4-(5-(4-(perfluoroethoxy)phenyl)-1,3,4-oxadiazol-2-yl)phenyl)urea

There total 8 articles about (Z)-1-(3-(2-isopropylphenyl)-4-oxothiazolidin-2-ylidene)-3-(4-(5-(4-(perfluoroethoxy)phenyl)-1,3,4-oxadiazol-2-yl)phenyl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1417885-18-7,1538587-92-6
C₂₇H₂₂F₅N₅O₃S

: 96-32-2
bromoacetic acid methyl ester

: 1417885-24-5
(Z)-1-(3-(2-isopropylphenyl)-4-oxothiazolidin-2-ylidene)-3-(4-(5-(4-(perfluoroethoxy)phenyl)-1,3,4-oxadiazol-2-yl)phenyl)urea

Guidance literature:: With sodium acetate; In ethanol; at 65 ℃; for 4h;

Reference yield:

: 1417885-87-0
ethyl 4-(perfluoroethoxy)benzoate

: 1417885-24-5
(Z)-1-(3-(2-isopropylphenyl)-4-oxothiazolidin-2-ylidene)-3-(4-(5-(4-(perfluoroethoxy)phenyl)-1,3,4-oxadiazol-2-yl)phenyl)urea

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrazine hydrate / ethanol / 36 h / 85 °C

2.1: acetic acid / 5 h / 120 °C

3.1: copper(l) iodide; caesium carbonate; 1,10-Phenanthroline / dimethyl sulfoxide / 18 h / 100 °C

4.1: sodium hydroxide / methanol / 42 h / 20 - 45 °C

5.1: triethylamine; diphenyl phosphoryl azide / isopropyl alcohol / 16 h / 20 °C

6.1: 1,2-dichloro-ethane / 3 h / 80 °C

6.2: 18 h / 20 °C

7.1: sodium acetate / 4 h / 65 °C

With copper(l) iodide; 1,10-Phenanthroline; diphenyl phosphoryl azide; sodium acetate; caesium carbonate; hydrazine hydrate; acetic acid; triethylamine; sodium hydroxide; In methanol; ethanol; dimethyl sulfoxide; 1,2-dichloro-ethane; isopropyl alcohol;

Reference yield:

: 56425-85-5
1-bromo-4-(pentafluoroethoxy)benzene

: 1417885-24-5
(Z)-1-(3-(2-isopropylphenyl)-4-oxothiazolidin-2-ylidene)-3-(4-(5-(4-(perfluoroethoxy)phenyl)-1,3,4-oxadiazol-2-yl)phenyl)urea

Guidance literature:: Multi-step reaction with 8 steps

1.1: TurboGrignard / tetrahydrofuran / 20 °C / Inert atmosphere; Cooling with ice

2.1: hydrazine hydrate / ethanol / 36 h / 85 °C

3.1: acetic acid / 5 h / 120 °C

4.1: copper(l) iodide; caesium carbonate; 1,10-Phenanthroline / dimethyl sulfoxide / 18 h / 100 °C

5.1: sodium hydroxide / methanol / 42 h / 20 - 45 °C

6.1: triethylamine; diphenyl phosphoryl azide / isopropyl alcohol / 16 h / 20 °C

7.1: 1,2-dichloro-ethane / 3 h / 80 °C

7.2: 18 h / 20 °C

8.1: sodium acetate / 4 h / 65 °C

With copper(l) iodide; TurboGrignard; 1,10-Phenanthroline; diphenyl phosphoryl azide; sodium acetate; caesium carbonate; hydrazine hydrate; acetic acid; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dimethyl sulfoxide; 1,2-dichloro-ethane; isopropyl alcohol;