C₂₃H₃₄O₄Si

Base Information

Chemical Name:C₂₃H₃₄O₄Si
CAS No.:1374991-74-8
Molecular Formula:C₂₃H₃₄O₄Si
Molecular Weight:402.606
Hs Code.:

C<sub>23</sub>H<sub>34</sub>O<sub>4</sub>Si

Synonyms:C₂₃H₃₄O₄Si

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Chemical Property of C₂₃H₃₄O₄Si

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Technology Process of C₂₃H₃₄O₄Si

There total 7 articles about C₂₃H₃₄O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1374991-67-9
(6S,7S)-6-(methoxymethoxy)-2,2,7,10,10,11,11-heptamethyl-3,3-diphenyl-4,9-dioxa-3,10-disiladodecane

: 1374991-74-8
C₂₃H₃₄O₄Si

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 15 ℃; for 0.5h; Cooling with ice;
DOI:10.1016/j.tetasy.2012.03.005

Reference yield:

: C₂₁H₂₈O₃Si

: 1374991-74-8
C₂₃H₃₄O₄Si

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

2: dmap; triethylamine / dichloromethane / 3 h / 0 - 20 °C

3: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 0 - 20 °C

4: toluene-4-sulfonic acid / methanol / 0.5 h / 15 °C / Cooling with ice

With dmap; sodium tetrahydroborate; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1016/j.tetasy.2012.03.005

Reference yield:

: C₁₃H₂₀O₅

: 1374991-74-8
C₂₃H₃₄O₄Si

Guidance literature:: Multi-step reaction with 11 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 2 h

2: water; acetic acid / 12 h / 20 °C

3: sodium periodate / methanol / 2 h / 0 - 20 °C

4: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

5: 1H-imidazole / dichloromethane / 0.25 h / 0 °C

6: boron trichloride / dichloromethane / 0.03 h / 0 °C

7: sodium periodate / methanol; water / 0.5 h / 0 °C

8: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

9: dmap; triethylamine / dichloromethane / 3 h / 0 - 20 °C

10: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 5 h / 0 - 20 °C

11: toluene-4-sulfonic acid / methanol / 0.5 h / 15 °C / Cooling with ice

With 1H-imidazole; dmap; sodium tetrahydroborate; sodium periodate; palladium 10% on activated carbon; water; hydrogen; boron trichloride; toluene-4-sulfonic acid; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; ethanol; dichloromethane; water;
DOI:10.1016/j.tetasy.2012.03.005