2-[2,7-Dichloro-5,8-dimethoxy-4-(2-nitro-phenyl)-quinolin-6-yl]-ethanol

Base Information

Chemical Name:2-[2,7-Dichloro-5,8-dimethoxy-4-(2-nitro-phenyl)-quinolin-6-yl]-ethanol
CAS No.:156489-09-7
Molecular Formula:C₁₉H₁₆Cl₂N₂O₅
Molecular Weight:423.252
Hs Code.:

Synonyms:2-[2,7-Dichloro-5,8-dimethoxy-4-(2-nitro-phenyl)-quinolin-6-yl]-ethanol

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Chemical Property of 2-[2,7-Dichloro-5,8-dimethoxy-4-(2-nitro-phenyl)-quinolin-6-yl]-ethanol

Chemical Property:

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Technology Process of 2-[2,7-Dichloro-5,8-dimethoxy-4-(2-nitro-phenyl)-quinolin-6-yl]-ethanol

There total 1 articles about 2-[2,7-Dichloro-5,8-dimethoxy-4-(2-nitro-phenyl)-quinolin-6-yl]-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 156489-08-6
Acetic acid 2-[2,7-dichloro-5,8-dimethoxy-4-(2-nitro-phenyl)-quinolin-6-yl]-ethyl ester

: 156489-09-7
2-[2,7-Dichloro-5,8-dimethoxy-4-(2-nitro-phenyl)-quinolin-6-yl]-ethanol

Guidance literature:: With potassium carbonate; In tetrahydrofuran; methanol; Yield given;
DOI:10.1021/jo00092a002

Reference yield: 81.0%

: 156489-09-7
2-[2,7-Dichloro-5,8-dimethoxy-4-(2-nitro-phenyl)-quinolin-6-yl]-ethanol

: 156489-10-0
[2,7-Dichloro-5,8-dimethoxy-4-(2-nitro-phenyl)-quinolin-6-yl]-acetaldehyde

Guidance literature:: With pyridine-SO₃ complex; In dimethyl sulfoxide;
DOI:10.1021/jo00092a002

Reference yield:

: 156489-09-7
2-[2,7-Dichloro-5,8-dimethoxy-4-(2-nitro-phenyl)-quinolin-6-yl]-ethanol

: 156489-12-2
N-{2-[2,7-Dichloro-5,8-dimethoxy-4-(2-nitro-phenyl)-quinolin-6-yl]-ethyl}-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / SO₃*Pyr / dimethylsulfoxide

2: 83 percent / H₂NSO₃H, pyridine / ethanol

3: MeOBH₂, 1M HCl / tetrahydrofuran

With pyridine; hydrogenchloride; methoxyborane; pyridine-SO₃ complex; aminosulfonic acid; In tetrahydrofuran; ethanol; dimethyl sulfoxide;
DOI:10.1021/jo00092a002