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Technology Process of N2C12H6(NC5H3C6H2(C2H5)2C6H4OCH2C6H4CH2N3)2

N2C12H6(NC5H3C6H2(C2H5)2C6H4OCH2C6H4CH2N3)2

Base Information
  • Chemical Name:N2C12H6(NC5H3C6H2(C2H5)2C6H4OCH2C6H4CH2N3)2
  • CAS No.:1147855-92-2
  • Molecular Formula:C70H60N10O2
  • Molecular Weight:1073.31
  • Hs Code.:
N<sub>2</sub>C<sub>12</sub>H<sub>6</sub>(NC<sub>5</sub>H<sub>3</sub>C<sub>6</sub>H<sub>2</sub>(C<sub>2</sub>H<sub>5</sub>)2C<sub>6</sub>H<sub>4</sub>OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>N<sub>3</sub>)2

Synonyms:N2C12H6(NC5H3C6H2(C2H5)2C6H4OCH2C6H4CH2N3)2

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Chemical Property of N2C12H6(NC5H3C6H2(C2H5)2C6H4OCH2C6H4CH2N3)2
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Technology Process of N2C12H6(NC5H3C6H2(C2H5)2C6H4OCH2C6H4CH2N3)2

There total 1 articles about N2C12H6(NC5H3C6H2(C2H5)2C6H4OCH2C6H4CH2N3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

C<sub>70</sub>H<sub>60</sub>Br<sub>2</sub>N<sub>4</sub>O<sub>2</sub>
1147855-90-0

C70H60Br2N4O2

N<sub>2</sub>C<sub>12</sub>H<sub>6</sub>(NC<sub>5</sub>H<sub>3</sub>C<sub>6</sub>H<sub>2</sub>(C<sub>2</sub>H<sub>5</sub>)2C<sub>6</sub>H<sub>4</sub>OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>N<sub>3</sub>)2
1147855-92-2

N2C12H6(NC5H3C6H2(C2H5)2C6H4OCH2C6H4CH2N3)2

Guidance literature:
With sodium azide; In N,N-dimethyl-formamide; at 80 ℃; for 20h; Inert atmosphere;

Reference yield: 99.0%

tetrakis(actonitrile)copper(I) hexafluorophosphate
64443-05-6

tetrakis(actonitrile)copper(I) hexafluorophosphate

((C(CH<sub>3</sub>)3)2C<sub>6</sub>H<sub>3</sub>)4C<sub>20</sub>H<sub>6</sub>N<sub>4</sub>ZnC<sub>8</sub>H<sub>2</sub>N<sub>4</sub>C<sub>10</sub>H<sub>4</sub>N<sub>2</sub>(C<sub>6</sub>H<sub>4</sub>(CH<sub>2</sub>)10O<sub>6</sub>C<sub>6</sub>H<sub>4</sub>)
1019647-90-5

((C(CH3)3)2C6H3)4C20H6N4ZnC8H2N4C10H4N2(C6H4(CH2)10O6C6H4)

N<sub>2</sub>C<sub>12</sub>H<sub>6</sub>(NC<sub>5</sub>H<sub>3</sub>C<sub>6</sub>H<sub>2</sub>(C<sub>2</sub>H<sub>5</sub>)2C<sub>6</sub>H<sub>4</sub>OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>N<sub>3</sub>)2
1147855-92-2

N2C12H6(NC5H3C6H2(C2H5)2C6H4OCH2C6H4CH2N3)2

2Zn<sup>(2+)</sup>*2Cu<sup>(1+)</sup>*2C<sub>116</sub>H<sub>124</sub>N<sub>10</sub>O<sub>6</sub><sup>(2-)</sup>*N<sub>2</sub>C<sub>12</sub>H<sub>6</sub>(N<sub>4</sub>C<sub>29</sub>H<sub>27</sub>O)2*2PF<sub>6</sub><sup>(1-)</sup>=(ZnC<sub>116</sub>H<sub>124</sub>N<sub>10</sub>O<sub>6</sub>)2Cu<sub>2</sub>(N<sub>2</sub>C<sub>12</sub>H<sub>6</sub>(N<sub>4</sub>C<sub>29</sub>H<sub>27</sub>O)2)(PF<sub>6</sub>)2

2Zn(2+)*2Cu(1+)*2C116H124N10O6(2-)*N2C12H6(N4C29H27O)2*2PF6(1-)=(ZnC116H124N10O6)2Cu2(N2C12H6(N4C29H27O)2)(PF6)2

Guidance literature:
In dichloromethane; acetonitrile; under Ar atm. to soln. Zn complex in CH2Cl2 soln. Cu complex in MeCN andstirred for 1 h in the absence of light at room temp., ligand in CH2Cl2 was added and stirred for 3 days in the absence of light; solvent was evapd.;
upstream raw materials:

C70H60Br2N4O2

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