4-{5-(2-hydroxyimino-1,1-dimethyl-propylamino)-3-[2-(2-hydroxyimino-1,1-dimethyl-propylamino)-ethyl]-pentylcarbamoyl}-thiobutyric acid 2,3,5,6-tetrafluoro-phenyl ester

Base Information

Chemical Name:4-{5-(2-hydroxyimino-1,1-dimethyl-propylamino)-3-[2-(2-hydroxyimino-1,1-dimethyl-propylamino)-ethyl]-pentylcarbamoyl}-thiobutyric acid 2,3,5,6-tetrafluoro-phenyl ester
CAS No.:489427-21-6
Molecular Formula:C₂₈H₄₃F₄N₅O₄S
Molecular Weight:621.74
Hs Code.:

4-{5-(2-hydroxyimino-1,1-dimethyl-propylamino)-3-[2-(2-hydroxyimino-1,1-dimethyl-propylamino)-ethyl]-pentylcarbamoyl}-thiobutyric acid 2,3,5,6-tetrafluoro-phenyl ester

Synonyms:4-{5-(2-hydroxyimino-1,1-dimethyl-propylamino)-3-[2-(2-hydroxyimino-1,1-dimethyl-propylamino)-ethyl]-pentylcarbamoyl}-thiobutyric acid 2,3,5,6-tetrafluoro-phenyl ester

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Chemical Property of 4-{5-(2-hydroxyimino-1,1-dimethyl-propylamino)-3-[2-(2-hydroxyimino-1,1-dimethyl-propylamino)-ethyl]-pentylcarbamoyl}-thiobutyric acid 2,3,5,6-tetrafluoro-phenyl ester

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Technology Process of 4-{5-(2-hydroxyimino-1,1-dimethyl-propylamino)-3-[2-(2-hydroxyimino-1,1-dimethyl-propylamino)-ethyl]-pentylcarbamoyl}-thiobutyric acid 2,3,5,6-tetrafluoro-phenyl ester

There total 13 articles about 4-{5-(2-hydroxyimino-1,1-dimethyl-propylamino)-3-[2-(2-hydroxyimino-1,1-dimethyl-propylamino)-ethyl]-pentylcarbamoyl}-thiobutyric acid 2,3,5,6-tetrafluoro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 460078-00-6
3-(2-aminoethyl)pentane-1,5-diamine

: 489427-21-6
4-{5-(2-hydroxyimino-1,1-dimethyl-propylamino)-3-[2-(2-hydroxyimino-1,1-dimethyl-propylamino)-ethyl]-pentylcarbamoyl}-thiobutyric acid 2,3,5,6-tetrafluoro-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / ethanol / 20 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide / 23 h

3.1: HATU; 4-methyl-morpholine / N,N-dimethyl-formamide / 0.08 h

3.2: 0.17 h

With 4-methyl-morpholine; potassium carbonate; HATU; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 37557-67-8
2-chloro-2-methyl-3-nitrosobutane

: 489427-21-6
4-{5-(2-hydroxyimino-1,1-dimethyl-propylamino)-3-[2-(2-hydroxyimino-1,1-dimethyl-propylamino)-ethyl]-pentylcarbamoyl}-thiobutyric acid 2,3,5,6-tetrafluoro-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / ethanol / 20 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide / 23 h

3.1: HATU; 4-methyl-morpholine / N,N-dimethyl-formamide / 0.08 h

3.2: 0.17 h

With 4-methyl-morpholine; potassium carbonate; HATU; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 87986-82-1
tris(2-acetoxyethyl)methane

: 489427-21-6
4-{5-(2-hydroxyimino-1,1-dimethyl-propylamino)-3-[2-(2-hydroxyimino-1,1-dimethyl-propylamino)-ethyl]-pentylcarbamoyl}-thiobutyric acid 2,3,5,6-tetrafluoro-phenyl ester

Guidance literature:: Multi-step reaction with 7 steps

1.1: ammonia / methanol / 80 °C

2.1: pyridine / dichloromethane / 24 h / 15 - 20 °C / Inert atmosphere

3.1: sodium azide / N,N-dimethyl-formamide / 24.5 h / 50 °C / Inert atmosphere; Cooling with ice

4.1: palladium 10% on activated carbon; hydrogen / water; ethanol / 12 h

5.1: potassium carbonate / ethanol / 20 °C / Inert atmosphere

6.1: N,N-dimethyl-formamide / 23 h

7.1: HATU; 4-methyl-morpholine / N,N-dimethyl-formamide / 0.08 h

7.2: 0.17 h

With 4-methyl-morpholine; pyridine; sodium azide; palladium 10% on activated carbon; ammonia; hydrogen; potassium carbonate; HATU; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;