methyl 2,3,4-O-tribenzoyl-α-L-[2'-13C]rhamnopyranosyl-(1->2)[2,3,4-O-tribenzoyl-α-L-[2''-13C]rhamnopyranosyl-(1->3)]-4-O-benzoyl-α-L-rhamnopyranoside

Base Information

Chemical Name:methyl 2,3,4-O-tribenzoyl-α-L-[2'-13C]rhamnopyranosyl-(1->2)[2,3,4-O-tribenzoyl-α-L-[2''-13C]rhamnopyranosyl-(1->3)]-4-O-benzoyl-α-L-rhamnopyranoside
CAS No.:1279715-22-8
Molecular Formula:C₆₈H₆₂O₂₀
Molecular Weight:1201.21
Hs Code.:

Synonyms:methyl 2,3,4-O-tribenzoyl-α-L-[2'-13C]rhamnopyranosyl-(1->2)[2,3,4-O-tribenzoyl-α-L-[2''-13C]rhamnopyranosyl-(1->3)]-4-O-benzoyl-α-L-rhamnopyranoside

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Chemical Property of methyl 2,3,4-O-tribenzoyl-α-L-[2'-13C]rhamnopyranosyl-(1->2)[2,3,4-O-tribenzoyl-α-L-[2''-13C]rhamnopyranosyl-(1->3)]-4-O-benzoyl-α-L-rhamnopyranoside

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Technology Process of methyl 2,3,4-O-tribenzoyl-α-L-[2'-13C]rhamnopyranosyl-(1->2)[2,3,4-O-tribenzoyl-α-L-[2''-13C]rhamnopyranosyl-(1->3)]-4-O-benzoyl-α-L-rhamnopyranoside

There total 3 articles about methyl 2,3,4-O-tribenzoyl-α-L-[2'-13C]rhamnopyranosyl-(1->2)[2,3,4-O-tribenzoyl-α-L-[2''-13C]rhamnopyranosyl-(1->3)]-4-O-benzoyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1279715-20-6
2,3,4-tri-O-benzoyl-α-L-[2-13C]rhamnopyranosyl bromide

: 69557-83-1
methyl-4-O-benzoyl-α-L-rhamnopyranoside

: 1279715-22-8
methyl 2,3,4-O-tribenzoyl-α-L-[2'-13C]rhamnopyranosyl-(1->2)[2,3,4-O-tribenzoyl-α-L-[2''-13C]rhamnopyranosyl-(1->3)]-4-O-benzoyl-α-L-rhamnopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; silver trifluoromethanesulfonate; In dichloromethane; at -40 - 20 ℃; Molecular sieve;
DOI:10.1002/mrc.2723

Reference yield:

: L-[2-13C]rhamnose

: 1279715-22-8
methyl 2,3,4-O-tribenzoyl-α-L-[2'-13C]rhamnopyranosyl-(1->2)[2,3,4-O-tribenzoyl-α-L-[2''-13C]rhamnopyranosyl-(1->3)]-4-O-benzoyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 20 - 60 °C

2: hydrogen bromide / acetic acid / 20 °C

3: 2,4,6-trimethyl-pyridine; silver trifluoromethanesulfonate / dichloromethane / -40 - 20 °C / Molecular sieve

With pyridine; 2,4,6-trimethyl-pyridine; hydrogen bromide; silver trifluoromethanesulfonate; In dichloromethane; acetic acid;
DOI:10.1002/mrc.2723

Reference yield:

: 98-88-4
benzoyl chloride

: 1279715-22-8
methyl 2,3,4-O-tribenzoyl-α-L-[2'-13C]rhamnopyranosyl-(1->2)[2,3,4-O-tribenzoyl-α-L-[2''-13C]rhamnopyranosyl-(1->3)]-4-O-benzoyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 20 - 60 °C

2: hydrogen bromide / acetic acid / 20 °C

3: 2,4,6-trimethyl-pyridine; silver trifluoromethanesulfonate / dichloromethane / -40 - 20 °C / Molecular sieve

With pyridine; 2,4,6-trimethyl-pyridine; hydrogen bromide; silver trifluoromethanesulfonate; In dichloromethane; acetic acid;
DOI:10.1002/mrc.2723