2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-buten-1-ol

Base Information

Chemical Name:2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-buten-1-ol
CAS No.:79936-91-7
Molecular Formula:C₁₄H₂₄O
Molecular Weight:211.32
Hs Code.:

Synonyms:2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-buten-1-ol

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Chemical Property of 2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-buten-1-ol

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Technology Process of 2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-buten-1-ol

There total 7 articles about 2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-buten-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 79936-88-2
2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-butencarbonsaureaethylester

: 79936-91-7
2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-buten-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 0.75h; -15 degC -> 0 degC;
DOI:10.1002/hlca.19810640504

Reference yield:

: 79936-78-0
(1'S,2'S,6'R)-2-methoxycarbonylmethyl-1,3-dimethyl-3-trideuteriomethyl-1-cyclohexancarbonsaure

: 79936-91-7
2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-buten-1-ol

Guidance literature:: Multi-step reaction with 3 steps

2: 82 percent / benzene / 17 h / Heating

3: 99 percent / LiAlH₄ / diethyl ether / 0.75 h / -15 degC -> 0 degC

With lithium aluminium tetrahydride; In diethyl ether; benzene;
DOI:10.1002/hlca.19810640504

Reference yield:

: 79936-76-8
C₂₀H₂₅⁽²⁾H₃O₂

: 79936-91-7
2-methyl-4<(1'S,6'R)-2',6'-dimethyl-6'-trideuteriomethyl-2'-cyclohexenyl>-(E)-2-buten-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1: conc. HCl / 1.17 h / Heating

2: 46 percent / MgSO₄, KMNO₄ / acetone / 2 h / Ambient temperature

4: 82 percent / benzene / 17 h / Heating

5: 99 percent / LiAlH₄ / diethyl ether / 0.75 h / -15 degC -> 0 degC

With hydrogenchloride; potassium permanganate; lithium aluminium tetrahydride; magnesium sulfate; In diethyl ether; acetone; benzene;
DOI:10.1002/hlca.19810640504