3-(4-benzyloxy-phenyl)-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propionamide

Base Information

Chemical Name:3-(4-benzyloxy-phenyl)-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propionamide
CAS No.:398125-99-0
Molecular Formula:C₂₄H₂₀N₂O₄
Molecular Weight:400.434
Hs Code.:

Synonyms:3-(4-benzyloxy-phenyl)-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propionamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-benzyloxy-phenyl)-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propionamide

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Technology Process of 3-(4-benzyloxy-phenyl)-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propionamide

There total 9 articles about 3-(4-benzyloxy-phenyl)-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2130-97-4
(S)-N^α-phthaloyl-O-benzyltyrosine

: 398125-99-0
3-(4-benzyloxy-phenyl)-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propionamide

Guidance literature:: (S)-N^α-phthaloyl-O-benzyltyrosine; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

With ammonia; In 1,4-dioxane; N,N-dimethyl-formamide; at 0 - 20 ℃; for 1.5h;

Reference yield: 73.0%

: O-benzyl-tyramine Hydrochloride

: 438470-19-0
methyl 2-(N-succinimidyloxycarbonyl)benzoate

: 398125-99-0
3-(4-benzyloxy-phenyl)-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propionamide

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 4h;
DOI:10.1021/jo016347h

Reference yield: 48.0%

: C₃₃H₂₅N₃O₄

: (S)-3-(1,3-dioxoisoindolin-2-yl)-1-azaspiro[4.5]deca-6,9-diene-2,8-dione

: 398125-99-0
3-(4-benzyloxy-phenyl)-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propionamide

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In water; at 60 ℃; for 2h; chemoselective reaction;
DOI:10.1021/acs.joc.9b01362