(1'R,2'S,5'R)-2'-(1-methyl-1-phenylethyl)-5'-methylcyclohexyl (R)-2-hydroxyphenylacetate

Base Information

Chemical Name:(1'R,2'S,5'R)-2'-(1-methyl-1-phenylethyl)-5'-methylcyclohexyl (R)-2-hydroxyphenylacetate
CAS No.:88292-43-7
Molecular Formula:C₂₄H₃₀O₃
Molecular Weight:366.5
Hs Code.:

Synonyms:(1'R,2'S,5'R)-2'-(1-methyl-1-phenylethyl)-5'-methylcyclohexyl (R)-2-hydroxyphenylacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1'R,2'S,5'R)-2'-(1-methyl-1-phenylethyl)-5'-methylcyclohexyl (R)-2-hydroxyphenylacetate

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Technology Process of (1'R,2'S,5'R)-2'-(1-methyl-1-phenylethyl)-5'-methylcyclohexyl (R)-2-hydroxyphenylacetate

There total 10 articles about (1'R,2'S,5'R)-2'-(1-methyl-1-phenylethyl)-5'-methylcyclohexyl (R)-2-hydroxyphenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 88002-15-7
Phenylglyoxylsaeure-<(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)-1-cyclohexyl>ester

: 71065-28-6,88292-43-7,139005-51-9
1R,2S,5R-(-)-8-phenylmenthyl mandelate

Guidance literature:: With samarium diiodide; water; In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1016/S0040-4039(01)00676-1

Reference yield: 48.0%

: 611-71-2
(R)-Mandelic Acid

: 65253-04-5
(-)-8-phenylmenthol

: 88292-43-7
(1'R,2'S,5'R)-2'-(1-methyl-1-phenylethyl)-5'-methylcyclohexyl (R)-2-hydroxyphenylacetate

Guidance literature:: With toluene-4-sulfonic acid; In toluene; Heating;
DOI:10.1021/jo00119a023

Reference yield:

: 65253-04-5
(-)-8-phenylmenthol

: 88292-43-7
(1'R,2'S,5'R)-2'-(1-methyl-1-phenylethyl)-5'-methylcyclohexyl (R)-2-hydroxyphenylacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / p-TsOH / toluene / Heating

2: 90 percent / toluene / Heating

3: 97 percent / Et₃N / CH₂Cl₂ / Ambient temperature

4: H₂O / rhodium(II) acetate / CH₂Cl₂ / Ambient temperature

With water; toluene-4-sulfonic acid; triethylamine; rhodium(II) acetate; In dichloromethane; toluene;
DOI:10.1021/jo00119a023