1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide selenide

Base Information

Chemical Name:1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide selenide
CAS No.:1620661-13-3
Molecular Formula:C₂₂H₃₉N₂OPSe
Molecular Weight:457.498
Hs Code.:

Synonyms:1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide selenide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide selenide

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Technology Process of 1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide selenide

There total 4 articles about 1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1569097-05-7
{[(di-tert-butylphosphoroselenoyl)(4-methoxyphenyl)amino]methylene}diisopropylammonium trifluoromethanesulfonate

: 1620661-13-3
1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide selenide

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at -90 - 20 ℃; for 1h;
DOI:10.1002/ejic.201402166

Reference yield: 76.0%

: 1620661-20-2
[(di-tert-butylphosphanyl)-4-methoxyphenylamino]diisopropylaminocarbene

: 1620661-13-3
1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide selenide

Guidance literature:: With selenium; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1002/ejic.201402166

Reference yield:

: 1569097-01-3
P,P-di-tert-butyl-N-(4-methoxyphenyl)phosphinoselenoic amide

: 1620661-13-3
1,1-di-tert-butyl-N,N-diisopropyl-N'-(4-methoxyphenyl)phosphanylcarboximidamide selenide

Guidance literature:: Multi-step reaction with 2 steps

1: 3 h / 0 - 20 °C

2: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -90 - 20 °C

With lithium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1002/ejic.201402166