1-{4-[7-(4-Acetyl-phenyl)-9,9-dipropyl-9H-fluoren-2-yl]-phenyl}-ethanone

Base Information

Chemical Name:1-{4-[7-(4-Acetyl-phenyl)-9,9-dipropyl-9H-fluoren-2-yl]-phenyl}-ethanone
CAS No.:204265-82-7
Molecular Formula:C₃₅H₃₄O₂
Molecular Weight:486.654
Hs Code.:

Synonyms:1-{4-[7-(4-Acetyl-phenyl)-9,9-dipropyl-9H-fluoren-2-yl]-phenyl}-ethanone

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Chemical Property of 1-{4-[7-(4-Acetyl-phenyl)-9,9-dipropyl-9H-fluoren-2-yl]-phenyl}-ethanone

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Technology Process of 1-{4-[7-(4-Acetyl-phenyl)-9,9-dipropyl-9H-fluoren-2-yl]-phenyl}-ethanone

There total 9 articles about 1-{4-[7-(4-Acetyl-phenyl)-9,9-dipropyl-9H-fluoren-2-yl]-phenyl}-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 75-36-5
acetyl chloride

: 111458-32-3
2,7-diphenyl-9,9-dipropylfluorene

: 204265-82-7
1-{4-[7-(4-Acetyl-phenyl)-9,9-dipropyl-9H-fluoren-2-yl]-phenyl}-ethanone

Guidance literature:: With aluminium trichloride; In dichloromethane; Heating;

Reference yield:

: 14966-05-3
9,9-diallylfluorene

: 204265-82-7
1-{4-[7-(4-Acetyl-phenyl)-9,9-dipropyl-9H-fluoren-2-yl]-phenyl}-ethanone

Guidance literature:: Multi-step reaction with 4 steps

1: 45 percent / H₂ / 5percent Pd/C / ethyl acetate / 4.5 h / 2280 Torr

2: 73 percent / Br₂ / CH₂Cl₂

3: 77 percent / PdCl₂(dppb) / tetrahydrofuran; diethyl ether / 24 h

4: 94 percent / AlCl₃ / CH₂Cl₂ / Heating

With aluminium trichloride; PdCl₂(PPh₂(CH₂)4PPh₂); hydrogen; bromine; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; ethyl acetate;

Reference yield:

: 86-73-7
9H-fluorene

: 204265-82-7
1-{4-[7-(4-Acetyl-phenyl)-9,9-dipropyl-9H-fluoren-2-yl]-phenyl}-ethanone

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / Br₂ / CH₂Cl₂

2: 88 percent / t-BuOK / dimethylformamide / 45 °C

3: 77 percent / PdCl₂(dppb) / tetrahydrofuran; diethyl ether / 24 h

4: 94 percent / AlCl₃ / CH₂Cl₂ / Heating

With aluminium trichloride; PdCl₂(PPh₂(CH₂)4PPh₂); potassium tert-butylate; bromine; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;