benzyl 2-benzamido-3-C-benzyloxycarbonyl-2,3,5-trideoxy-α-D-ribofuranoside

Base Information

Chemical Name:benzyl 2-benzamido-3-C-benzyloxycarbonyl-2,3,5-trideoxy-α-D-ribofuranoside
CAS No.:119447-63-1
Molecular Formula:C₂₇H₂₇NO₅
Molecular Weight:445.515
Hs Code.:

Synonyms:benzyl 2-benzamido-3-C-benzyloxycarbonyl-2,3,5-trideoxy-α-D-ribofuranoside

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Chemical Property of benzyl 2-benzamido-3-C-benzyloxycarbonyl-2,3,5-trideoxy-α-D-ribofuranoside

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Technology Process of benzyl 2-benzamido-3-C-benzyloxycarbonyl-2,3,5-trideoxy-α-D-ribofuranoside

There total 4 articles about benzyl 2-benzamido-3-C-benzyloxycarbonyl-2,3,5-trideoxy-α-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.6%

: 98-88-4
benzoyl chloride

: 117996-81-3
benzyl 2-amino-3-C-benzyloxycarbonyl-2,3,5-trideoxy-α-D-ribofuranoside

: 119447-63-1
benzyl 2-benzamido-3-C-benzyloxycarbonyl-2,3,5-trideoxy-α-D-ribofuranoside

Guidance literature:: With ethyl azide; In dichloromethane; for 0.0833333h; Ambient temperature;
DOI:10.1271/bbb1961.52.2027

Reference yield:

: (1S,2R,4R,5R)-6-(2,4-dimethoxybenzyl)-4-hydroxy-2-methyl-3-oxa-6-azabicyclo<3.2.0>heptan-7-one

: 119447-63-1
benzyl 2-benzamido-3-C-benzyloxycarbonyl-2,3,5-trideoxy-α-D-ribofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 30.3 percent / HCl / Ambient temperature

2: 80.4 percent / CAN / acetone; H₂O / 0.08 h / Ambient temperature

3: 94.6 percent / EtN₃ / CH₂Cl₂ / 0.08 h / Ambient temperature

With hydrogenchloride; ammonium cerium(IV) nitrate; ethyl azide; In dichloromethane; water; acetone;
DOI:10.1271/bbb1961.52.2027

Reference yield:

: 117996-84-6
benzyl 3-C-benzyloxycarbonyl-2-(2,4-dimethoxybenzylamino)-2,3,5-trideoxy-α-D-ribofuranoside

: 119447-63-1
benzyl 2-benzamido-3-C-benzyloxycarbonyl-2,3,5-trideoxy-α-D-ribofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 80.4 percent / CAN / acetone; H₂O / 0.08 h / Ambient temperature

2: 94.6 percent / EtN₃ / CH₂Cl₂ / 0.08 h / Ambient temperature

With ammonium cerium(IV) nitrate; ethyl azide; In dichloromethane; water; acetone;
DOI:10.1271/bbb1961.52.2027