Technology Process of C18H27NO3
There total 1 articles about C18H27NO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 3 steps
1: palladium on activated charcoal / ethanol / 12 h / 20 °C / Inert atmosphere
2: hydrogen bromide; acetic acid / water / 12 h / Reflux
3: sodium iodide; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / acetonitrile / 48 h / Inert atmosphere; Reflux
With
palladium on activated charcoal; hydrogen bromide; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; acetic acid; sodium iodide;
In
ethanol; water; acetonitrile;
- Guidance literature:
-
In
toluene;
for 48h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: trifluoroacetic acid / 4 h / 100 °C / Sealed tube
2: triethylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
3: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 20.5 h / 20 - 100 °C / Inert atmosphere; Schlenk technique
With
palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; trifluoroacetic acid;
In
N,N-dimethyl-formamide; toluene;