(1S,3S,4R)-2-[(S)-1-phenylethyl]-3-(aminomethyl)-2-azabicyclo[2,2,1]heptane

Base Information

Chemical Name:(1S,3S,4R)-2-[(S)-1-phenylethyl]-3-(aminomethyl)-2-azabicyclo[2,2,1]heptane
CAS No.:1290085-13-0
Molecular Formula:C₁₅H₂₂N₂
Molecular Weight:230.353
Hs Code.:

Synonyms:(1S,3S,4R)-2-[(S)-1-phenylethyl]-3-(aminomethyl)-2-azabicyclo[2,2,1]heptane

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Chemical Property of (1S,3S,4R)-2-[(S)-1-phenylethyl]-3-(aminomethyl)-2-azabicyclo[2,2,1]heptane

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Technology Process of (1S,3S,4R)-2-[(S)-1-phenylethyl]-3-(aminomethyl)-2-azabicyclo[2,2,1]heptane

There total 5 articles about (1S,3S,4R)-2-[(S)-1-phenylethyl]-3-(aminomethyl)-2-azabicyclo[2,2,1]heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: C₁₅H₁₉NO

: 1290085-13-0
(1S,3S,4R)-2-[(S)-1-phenylethyl]-3-(aminomethyl)-2-azabicyclo[2,2,1]heptane

Guidance literature:: C₁₅H₁₉NO; With hydroxylamine hydrochloride;

With lithium aluminium tetrahydride;
DOI:10.1039/c6nj02251k

Reference yield: 56.0%

: 1290085-10-7
(1S,3S,4R)-2-[(S)-1-phenylethyl]-3-(azidomethyl)-2-azabicyclo[2,2,1]heptane

: 1290085-13-0
(1S,3S,4R)-2-[(S)-1-phenylethyl]-3-(aminomethyl)-2-azabicyclo[2,2,1]heptane

Guidance literature:: With triphenylphosphine; In methanol; Reflux;
DOI:10.1016/j.tetasy.2010.12.011

Reference yield:

: 1290085-07-2
(1S,3S,4R)-2-[(S)-1-phenylethyl]-3-hydroxymethyl-2-azabicyclo[2,2,1]heptane

: 1290085-13-0
(1S,3S,4R)-2-[(S)-1-phenylethyl]-3-(aminomethyl)-2-azabicyclo[2,2,1]heptane

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia; triphenylphosphine; diethylazodicarboxylate / toluene; benzene / Cooling with ice; Inert atmosphere

2: triphenylphosphine / methanol / Reflux

With ammonia; triphenylphosphine; diethylazodicarboxylate; In methanol; toluene; benzene;
DOI:10.1016/j.tetasy.2010.12.011