(S)-O-(tert-butyldimethylsilyl)-N-(p-toluenesulfonyl)-tert-butylglycinol

Base Information

Chemical Name:(S)-O-(tert-butyldimethylsilyl)-N-(p-toluenesulfonyl)-tert-butylglycinol
CAS No.:903516-21-2
Molecular Formula:C₁₉H₃₅NO₃SSi
Molecular Weight:385.643
Hs Code.:

Synonyms:(S)-O-(tert-butyldimethylsilyl)-N-(p-toluenesulfonyl)-tert-butylglycinol

Suppliers and Price of (S)-O-(tert-butyldimethylsilyl)-N-(p-toluenesulfonyl)-tert-butylglycinol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-O-(tert-butyldimethylsilyl)-N-(p-toluenesulfonyl)-tert-butylglycinol

Chemical Property:

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Technology Process of (S)-O-(tert-butyldimethylsilyl)-N-(p-toluenesulfonyl)-tert-butylglycinol

There total 3 articles about (S)-O-(tert-butyldimethylsilyl)-N-(p-toluenesulfonyl)-tert-butylglycinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 887255-41-6
(S)-(+)-N-(1-hydroxymethyl-2,2-dimethylpropyl)-4-methylbenzenesulfonamide

: 18162-48-6
tert-butyldimethylsilyl chloride

: 903516-21-2
(S)-O-(tert-butyldimethylsilyl)-N-(p-toluenesulfonyl)-tert-butylglycinol

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 - 25 ℃;
DOI:10.1021/jo060495w

Reference yield:

: 112245-13-3
(S)-tert-leucinol

: 903516-21-2
(S)-O-(tert-butyldimethylsilyl)-N-(p-toluenesulfonyl)-tert-butylglycinol

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / DMAP; triethylamine / CH₂Cl₂ / 0 - 25 °C

2: 99 percent / imidazole / dimethylformamide / 0 - 25 °C

With 1H-imidazole; dmap; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo060495w

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 903516-21-2
(S)-O-(tert-butyldimethylsilyl)-N-(p-toluenesulfonyl)-tert-butylglycinol

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / DMAP; triethylamine / CH₂Cl₂ / 0 - 25 °C

2: 99 percent / imidazole / dimethylformamide / 0 - 25 °C

With 1H-imidazole; dmap; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo060495w