benzyl N-ferrocenylcarbamate

Base Information

Chemical Name:benzyl N-ferrocenylcarbamate
CAS No.:98639-14-6
Molecular Formula:C₁₈H₁₇FeNO₂
Molecular Weight:335.185
Hs Code.:

Synonyms:benzyl N-ferrocenylcarbamate

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Chemical Property of benzyl N-ferrocenylcarbamate

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Technology Process of benzyl N-ferrocenylcarbamate

There total 4 articles about benzyl N-ferrocenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: ferrocenoyl azide

: 100-51-6,185532-71-2
benzyl alcohol

: 98639-14-6
benzyl N-ferrocenylcarbamate

Guidance literature:: In toluene; for 2h; Inert atmosphere; Reflux;
DOI:10.1039/c7ob00211d

Reference yield: 86.0%

: C₁₀H₉FeNHCONHCH(COOC₂H₅)CH₂CH(CH₃)2

: 98639-14-6
benzyl N-ferrocenylcarbamate

Guidance literature:: With sodium hydroxide; In ethanol; water;
DOI:10.1007/BF00900170

Reference yield: 55.0%

: 1271-42-7
ferrocenecarboxylic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 98639-14-6
benzyl N-ferrocenylcarbamate

Guidance literature:: With NaN₃; (C₄H₉)4NBr; N,N-dimethylchlorosulfitomethaniminium chloride; In dichloromethane; under Ar or N2, Schlenk setup, ferrocenylcarboxylic acid (5.43 mmol) mixed with Bu4NBr (1.1 mmol) and NaN3 (11 mmol) treated with CH2Cl2 and pyridine (16.5 mmol), N,N-dimethylchlorosulfitomethaniminium chloride added, stirred for 1 h, benzylic alcohol..; concd., chromd. (SiO2, CH2Cl2+1% Et3N), elem. anal.;
DOI:10.1002/ejic.200400691