N₂-isobutyryl-5'-O-(4,4'-dimethoxytrityl)-2'-methylseleno-2'-deoxyguanosine 3'-(2-cyanoethyl)-N,N-diisopropylphosphoramidite

Base Information

• Chemical Name: N₂-isobutyryl-5'-O-(4,4'-dimethoxytrityl)-2'-methylseleno-2'-deoxyguanosine 3'-(2-cyanoethyl)-N,N-diisopropylphosphoramidite
• CAS No.: 1206198-31-3
• Molecular Formula: C₄₅H₅₆N₇O₈PSe
• Molecular Weight: 932.916

Synonyms:N₂-isobutyryl-5'-O-(4,4'-dimethoxytrityl)-2'-methylseleno-2'-deoxyguanosine 3'-(2-cyanoethyl)-N,N-diisopropylphosphoramidite

Chemical Property of N₂-isobutyryl-5'-O-(4,4'-dimethoxytrityl)-2'-methylseleno-2'-deoxyguanosine 3'-(2-cyanoethyl)-N,N-diisopropylphosphoramidite

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Technology Process of N₂-isobutyryl-5'-O-(4,4'-dimethoxytrityl)-2'-methylseleno-2'-deoxyguanosine 3'-(2-cyanoethyl)-N,N-diisopropylphosphoramidite

There total 1 articles about N₂-isobutyryl-5'-O-(4,4'-dimethoxytrityl)-2'-methylseleno-2'-deoxyguanosine 3'-(2-cyanoethyl)-N,N-diisopropylphosphoramidite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

N2-isobutyryl-5'-O-(4,4'-dimethoxytrityl)-2'-methylseleno-2'-deoxyguanosine (1206198-30-2) + 2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine (124482-92-4,89992-70-1) → N2-isobutyryl-5'-O-(4,4'-dimethoxytrityl)-2'-methylseleno-2'-deoxyguanosine 3'-(2-cyanoethyl)-N,N-diisopropylphosphoramidite (1206198-31-3)

Guidance literature:

N₂-isobutyryl-5'-O-(4,4'-dimethoxytrityl)-2'-methylseleno-2'-deoxyguanosine; With N,N-dimethyl-ethanamine; In dichloromethane; for 0.166667h; Inert atmosphere;

2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jo902190c

upstream raw materials:

N₂-isobutyryl-5'-O-(4,4'-dimethoxytrityl)-2'-methylseleno-2'-deoxyguanosine

2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

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