{6-[(1-methoxy-2-phenylindolizin-3-yl)carbonyl]-2,4-dioxo-1,4-dihydroquinazolin-3(2H)-yl}acetic acid sodium salt

Base Information

Chemical Name:{6-[(1-methoxy-2-phenylindolizin-3-yl)carbonyl]-2,4-dioxo-1,4-dihydroquinazolin-3(2H)-yl}acetic acid sodium salt
CAS No.:1354708-74-9
Molecular Formula:C₂₆H₁₈N₃O₆*Na
Molecular Weight:491.435
Hs Code.:

Synonyms:{6-[(1-methoxy-2-phenylindolizin-3-yl)carbonyl]-2,4-dioxo-1,4-dihydroquinazolin-3(2H)-yl}acetic acid sodium salt

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Chemical Property of {6-[(1-methoxy-2-phenylindolizin-3-yl)carbonyl]-2,4-dioxo-1,4-dihydroquinazolin-3(2H)-yl}acetic acid sodium salt

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Technology Process of {6-[(1-methoxy-2-phenylindolizin-3-yl)carbonyl]-2,4-dioxo-1,4-dihydroquinazolin-3(2H)-yl}acetic acid sodium salt

There total 6 articles about {6-[(1-methoxy-2-phenylindolizin-3-yl)carbonyl]-2,4-dioxo-1,4-dihydroquinazolin-3(2H)-yl}acetic acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354708-75-0
ethyl {6-[(1-methoxy-2-phenylindolizin-3-yl)carbonyl]-2,4-dioxo-1,4-dihydroquinazolin-3(2H)-yl}acetate

: 1354708-74-9
{6-[(1-methoxy-2-phenylindolizin-3-yl)carbonyl]-2,4-dioxo-1,4-dihydroquinazolin-3(2H)-yl}acetic acid sodium salt

Guidance literature:: With water; sodium hydroxide; In methanol; for 7h; Reflux;

Reference yield:

: 1354709-83-3
6-[(1-methoxy-2-phenylindolizin-3-yl)carbonyl]-2-phenyl-4H-3,1-benzoxazin-4-one

: 1354708-74-9
{6-[(1-methoxy-2-phenylindolizin-3-yl)carbonyl]-2,4-dioxo-1,4-dihydroquinazolin-3(2H)-yl}acetic acid sodium salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide; water / 1-methyl-pyrrolidin-2-one / 24 h / 80 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

3.1: 1,4-dioxane / 1 h / 20 °C / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

4.1: sodium hydroxide; water / methanol / 7 h / Reflux

With water; caesium carbonate; potassium hydroxide; sodium hydroxide; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; N,N-dimethyl-formamide;

Reference yield:

: 1354709-85-5
methyl 2-amino-5-[(1-methoxy-2-phenylindolizin-3-yl)carbonyl]benzoate

: 1354708-74-9
{6-[(1-methoxy-2-phenylindolizin-3-yl)carbonyl]-2,4-dioxo-1,4-dihydroquinazolin-3(2H)-yl}acetic acid sodium salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,4-dioxane / 1 h / 20 °C / Inert atmosphere

1.2: 2 h / 20 °C / Inert atmosphere

2.1: sodium hydroxide; water / methanol / 7 h / Reflux

With water; sodium hydroxide; In 1,4-dioxane; methanol;