2,6-dibenzyl-1H,5H-[1,4]dithiino[2,3-c:5,6-c']dipyrrole-1,3,5,7(2H,6H)-tetrone

Base Information

Chemical Name:2,6-dibenzyl-1H,5H-[1,4]dithiino[2,3-c:5,6-c']dipyrrole-1,3,5,7(2H,6H)-tetrone
CAS No.:16114-38-8
Molecular Formula:C₂₂H₁₄N₂O₄S₂
Molecular Weight:434.496
Hs Code.:

Synonyms:2,6-dibenzyl-1H,5H-[1,4]dithiino[2,3-c:5,6-c']dipyrrole-1,3,5,7(2H,6H)-tetrone

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Chemical Property of 2,6-dibenzyl-1H,5H-[1,4]dithiino[2,3-c:5,6-c']dipyrrole-1,3,5,7(2H,6H)-tetrone

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Technology Process of 2,6-dibenzyl-1H,5H-[1,4]dithiino[2,3-c:5,6-c']dipyrrole-1,3,5,7(2H,6H)-tetrone

There total 4 articles about 2,6-dibenzyl-1H,5H-[1,4]dithiino[2,3-c:5,6-c']dipyrrole-1,3,5,7(2H,6H)-tetrone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 16114-24-2
1-benzyl-3,4-dichloro-pyrrole-2,5-dione

: 16114-38-8
2,6-dibenzyl-1H,5H-[1,4]dithiino[2,3-c:5,6-c']dipyrrole-1,3,5,7(2H,6H)-tetrone

Guidance literature:: With thiourea; In ethanol; at 80 ℃; for 1.5h;
DOI:10.1021/acs.cgd.9b01167

Reference yield: 60.0%

: 64984-60-7
4-oxo-4-[(phenylmethyl)amino]butanoic acid

: 16114-38-8
2,6-dibenzyl-1H,5H-[1,4]dithiino[2,3-c:5,6-c']dipyrrole-1,3,5,7(2H,6H)-tetrone

Guidance literature:: With thionyl chloride; In 1,4-dioxane; at 20 - 50 ℃; Inert atmosphere;
DOI:10.1002/jhet.305

Reference yield:

: 100-46-9
benzylamine

: 16114-38-8
2,6-dibenzyl-1H,5H-[1,4]dithiino[2,3-c:5,6-c']dipyrrole-1,3,5,7(2H,6H)-tetrone

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / dioxane / 0.5 h / 80 °C

2: thionyl chloride / dioxane / 6 h / 20 °C

With thionyl chloride; In 1,4-dioxane;
DOI:10.1080/00397910600943600