2-acetamido-5--4-diazocyclohexadien-1-one

Base Information

Chemical Name:2-acetamido-5--4-diazocyclohexadien-1-one
CAS No.:106994-11-0
Molecular Formula:C₁₂H₁₄N₄O₄S
Molecular Weight:310.334
Hs Code.:

2-acetamido-5-<N-(2-propenyl)methanesulfonamido>-4-diazocyclohexadien-1-one

Synonyms:2-acetamido-5--4-diazocyclohexadien-1-one

Suppliers and Price of 2-acetamido-5--4-diazocyclohexadien-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-acetamido-5--4-diazocyclohexadien-1-one

Chemical Property:

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Technology Process of 2-acetamido-5--4-diazocyclohexadien-1-one

There total 9 articles about 2-acetamido-5--4-diazocyclohexadien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 116911-54-7
N-[4-(Allyl-methanesulfonyl-amino)-5-amino-2-hydroxy-phenyl]-acetamide; hydrochloride

: 106994-11-0
2-acetamido-5--4-diazocyclohexadien-1-one

Guidance literature:: With isopentyl nitrite; In ethanol; at 0 - 25 ℃; for 0.75h;
DOI:10.1021/jo00256a036

Reference yield:

: 25945-95-3
N-<2-(benzyloxy)-4-nitrophenyl>acetamide

: 106994-11-0
2-acetamido-5--4-diazocyclohexadien-1-one

Guidance literature:: Multi-step reaction with 6 steps

1: Zn / ethanol

2: pyridine

3: HNO₃, Hg(OAc)2 / acetic anhydride

4: KOC(CH₃)3 / dimethylformamide

5: BBr₃

6: 1.) Zn; 2.) HCl, i-C₅H₁₁ONO / 1.) EtOH; 2.) MeOH

With hydrogenchloride; potassium tert-butylate; mercury(II) diacetate; nitric acid; boron tribromide; zinc; isopentyl nitrite; In pyridine; ethanol; acetic anhydride; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)84617-1

Reference yield:

: 25351-89-7
N-(2-hydroxy-4-nitrophenyl)acetamide

: 106994-11-0
2-acetamido-5--4-diazocyclohexadien-1-one

Guidance literature:: Multi-step reaction with 7 steps

1: K₂CO₃, KI

2: Zn / ethanol

3: pyridine

4: HNO₃, Hg(OAc)2 / acetic anhydride

5: KOC(CH₃)3 / dimethylformamide

6: BBr₃

7: 1.) Zn; 2.) HCl, i-C₅H₁₁ONO / 1.) EtOH; 2.) MeOH

With hydrogenchloride; potassium tert-butylate; mercury(II) diacetate; nitric acid; boron tribromide; potassium carbonate; potassium iodide; zinc; isopentyl nitrite; In pyridine; ethanol; acetic anhydride; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)84617-1