2-amino-6-O-benzyl-9-{5'-O-benzyl-3-O-[2'',6''-di-O-benzyl-α-D-glucopyranosyl]-β-D-ribofuranosyl}purine

Base Information

Chemical Name:2-amino-6-O-benzyl-9-{5'-O-benzyl-3-O-[2'',6''-di-O-benzyl-α-D-glucopyranosyl]-β-D-ribofuranosyl}purine
CAS No.:897364-69-1
Molecular Formula:C₄₄H₄₇N₅O₁₀
Molecular Weight:805.885
Hs Code.:

Synonyms:2-amino-6-O-benzyl-9-{5'-O-benzyl-3-O-[2'',6''-di-O-benzyl-α-D-glucopyranosyl]-β-D-ribofuranosyl}purine

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Chemical Property of 2-amino-6-O-benzyl-9-{5'-O-benzyl-3-O-[2'',6''-di-O-benzyl-α-D-glucopyranosyl]-β-D-ribofuranosyl}purine

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Technology Process of 2-amino-6-O-benzyl-9-{5'-O-benzyl-3-O-[2'',6''-di-O-benzyl-α-D-glucopyranosyl]-β-D-ribofuranosyl}purine

There total 2 articles about 2-amino-6-O-benzyl-9-{5'-O-benzyl-3-O-[2'',6''-di-O-benzyl-α-D-glucopyranosyl]-β-D-ribofuranosyl}purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 897364-66-8
2-amino-6-chloro-9-[2'-O-acetyl-5'-O-benzyl-3'-O-(3'',4''-di-O-acetyl-2'',6''-di-O-benzyl-α-D-glucopyranosyl)-β-D-ribofuranosyl]purine

: 100-51-6,185532-71-2
benzyl alcohol

: 897364-69-1
2-amino-6-O-benzyl-9-{5'-O-benzyl-3-O-[2'',6''-di-O-benzyl-α-D-glucopyranosyl]-β-D-ribofuranosyl}purine

Guidance literature:: With sodium hydride; at 120 ℃;
DOI:10.1021/jo702617c

Reference yield: 43.0%

: 897364-66-8
2-amino-6-chloro-9-[2'-O-acetyl-5'-O-benzyl-3'-O-(3'',4''-di-O-acetyl-2'',6''-di-O-benzyl-α-D-glucopyranosyl)-β-D-ribofuranosyl]purine

: 100-51-6,185532-71-2
benzyl alcohol

: 897364-70-4
C₂₄H₂₅N₅O₅

: 897364-69-1
2-amino-6-O-benzyl-9-{5'-O-benzyl-3-O-[2'',6''-di-O-benzyl-α-D-glucopyranosyl]-β-D-ribofuranosyl}purine

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 80 ℃; for 3h;
DOI:10.1039/b517911d

Reference yield: 82.0%

: 897364-69-1
2-amino-6-O-benzyl-9-{5'-O-benzyl-3-O-[2'',6''-di-O-benzyl-α-D-glucopyranosyl]-β-D-ribofuranosyl}purine

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 897364-71-5
2-amino-6-O-benzyl-9-{5'-O-benzyl-2'-O-(dibenzyloxyphosphoryl)-3'-O-[2'',6''-di-O-benzyl-3'',4''-bis-(dibenzyloxyphosphoryl)-α-D-glucopyranosyl]-β-D-ribofuranosyl}purine

Guidance literature:: 2-amino-6-O-benzyl-9-{5'-O-benzyl-3-O-[2'',6''-di-O-benzyl-α-D-glucopyranosyl]-β-D-ribofuranosyl}purine; Dibenzyl N,N-diisopropylphosphoramidite; With imidazole trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 0.75h;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - 20 ℃; for 1.5h; Further stages.;
DOI:10.1021/jo702617c