N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[6-O-{methyl 2,3-diazido-4-O-tert-butyldimethylsilyl-2,3-dideoxy-β-D-mannopyranosyl uronate}-2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

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Chemical Name:N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[6-O-{methyl 2,3-diazido-4-O-tert-butyldimethylsilyl-2,3-dideoxy-β-D-mannopyranosyl uronate}-2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside
CAS No.:1319717-50-4
Molecular Formula:C₈₁H₁₀₈N₁₆O₂₀Si₂
Molecular Weight:1682.01
Hs Code.:

N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[6-O-{methyl 2,3-diazido-4-O-tert-butyldimethylsilyl-2,3-dideoxy-β-D-mannopyranosyl uronate}-2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

Synonyms:N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[6-O-{methyl 2,3-diazido-4-O-tert-butyldimethylsilyl-2,3-dideoxy-β-D-mannopyranosyl uronate}-2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

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Chemical Property of N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[6-O-{methyl 2,3-diazido-4-O-tert-butyldimethylsilyl-2,3-dideoxy-β-D-mannopyranosyl uronate}-2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

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Technology Process of N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[6-O-{methyl 2,3-diazido-4-O-tert-butyldimethylsilyl-2,3-dideoxy-β-D-mannopyranosyl uronate}-2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

There total 1 articles about N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[6-O-{methyl 2,3-diazido-4-O-tert-butyldimethylsilyl-2,3-dideoxy-β-D-mannopyranosyl uronate}-2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1319717-49-1
methyl (phenyl 2,3-diazido-4-O-tert-butyldimethylsilyl-2,3-dideoxy-1-thio-β-D-mannopyranosyl uronate)

: 1319717-48-0
N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

: 1319717-50-4
N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[6-O-{methyl 2,3-diazido-4-O-tert-butyldimethylsilyl-2,3-dideoxy-β-D-mannopyranosyl uronate}-2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

Guidance literature:: methyl (phenyl 2,3-diazido-4-O-tert-butyldimethylsilyl-2,3-dideoxy-1-thio-β-D-mannopyranosyl uronate); With tri-tert-butyl phosphine; 1,1'-sulfinylbisbenzene; In dichloromethane; toluene; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With trifluoromethylsulfonic anhydride; In dichloromethane; toluene; at -80 ℃; for 0.333333h;

N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside; In dichloromethane; toluene; at -30 - -10 ℃;
DOI:10.1021/jo201179p