N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

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Chemical Name:N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside
CAS No.:1319717-48-0
Molecular Formula:C₆₈H₈₆N₁₀O₁₆Si
Molecular Weight:1327.57
Hs Code.:

N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

Synonyms:N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

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Chemical Property of N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

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Technology Process of N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

There total 1 articles about N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1319717-47-9
N-(benzyl)benzyloxycarbonyl-5-aminopentyl O-(methyl 4-O-[2,3,4-tri-O-benzyl-6-O-{9-fluorenylmethoxycarbonyl}-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

: 1319717-48-0
N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

Guidance literature:: With pyridine; triethylamine; for 3h;
DOI:10.1021/jo201179p

Reference yield: 74.0%

: 1319717-49-1
methyl (phenyl 2,3-diazido-4-O-tert-butyldimethylsilyl-2,3-dideoxy-1-thio-β-D-mannopyranosyl uronate)

: 1319717-48-0
N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

: 1319717-50-4
N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[6-O-{methyl 2,3-diazido-4-O-tert-butyldimethylsilyl-2,3-dideoxy-β-D-mannopyranosyl uronate}-2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside

Guidance literature:: methyl (phenyl 2,3-diazido-4-O-tert-butyldimethylsilyl-2,3-dideoxy-1-thio-β-D-mannopyranosyl uronate); With tri-tert-butyl phosphine; 1,1'-sulfinylbisbenzene; In dichloromethane; toluene; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With trifluoromethylsulfonic anhydride; In dichloromethane; toluene; at -80 ℃; for 0.333333h;

N-(benzyl)benzyloxycarbonyl-5-aminopentyl 3-O-(methyl 4-O-[2,3,4-tri-O-benzyl-α-D-glucopyranosyl]-2,3-diazido-2,3-dideoxy-β-D-mannopyranosyl uronate)-2-azido-4,6-O-di-tert-butylsilylidene-2-deoxy-α-D-glucopyranoside; In dichloromethane; toluene; at -30 - -10 ℃;
DOI:10.1021/jo201179p