(2S)-4-[(5-chloro-2-hydroxy-3-sulfophenyl)carbamoyl]-2-(dimethylamino)butanoic acid

Base Information

Chemical Name:(2S)-4-[(5-chloro-2-hydroxy-3-sulfophenyl)carbamoyl]-2-(dimethylamino)butanoic acid
CAS No.:1333219-13-8
Molecular Formula:C₁₃H₁₇ClN₂O₇S
Molecular Weight:380.806
Hs Code.:

Synonyms:(2S)-4-[(5-chloro-2-hydroxy-3-sulfophenyl)carbamoyl]-2-(dimethylamino)butanoic acid

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Chemical Property of (2S)-4-[(5-chloro-2-hydroxy-3-sulfophenyl)carbamoyl]-2-(dimethylamino)butanoic acid

Chemical Property:

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Technology Process of (2S)-4-[(5-chloro-2-hydroxy-3-sulfophenyl)carbamoyl]-2-(dimethylamino)butanoic acid

There total 2 articles about (2S)-4-[(5-chloro-2-hydroxy-3-sulfophenyl)carbamoyl]-2-(dimethylamino)butanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1220125-05-2
(2S)-2-amino-4-[(5-chloro-2-hydroxy-3-sulfophenyl)carbamoyl]butanoic acid

: 1333219-13-8
(2S)-4-[(5-chloro-2-hydroxy-3-sulfophenyl)carbamoyl]-2-(dimethylamino)butanoic acid

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In water;

Reference yield:

: 88-23-3
2-amino-4-chlorophenol-6-sulfonic acid

: 24277-39-2
N-tert-butoxycarbonyl glutamic acid tert-butyl ester

: 1333219-13-8
(2S)-4-[(5-chloro-2-hydroxy-3-sulfophenyl)carbamoyl]-2-(dimethylamino)butanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-hydroxy-7-aza-benzotriazole; pyridine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C

1.2: 1.5 h / 20 °C

2.1: hydrogen; palladium 10% on activated carbon / water

With pyridine; 1-hydroxy-7-aza-benzotriazole; palladium 10% on activated carbon; hydrogen; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In water; N,N-dimethyl-formamide;