1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 4-methoxyphenylborane complex

Base Information

• Chemical Name: 1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 4-methoxyphenylborane complex
• CAS No.: 1312175-69-1
• Molecular Formula: C₃₄H₄₅BN₂O
• Molecular Weight: 508.555

Synonyms:1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 4-methoxyphenylborane complex

Chemical Property of 1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 4-methoxyphenylborane complex

Chemical Property:

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Technology Process of 1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 4-methoxyphenylborane complex

There total 1 articles about 1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 4-methoxyphenylborane complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

4-methoxyphenylboronic acid (5720-07-0) + 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene (244187-81-3) → 1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 4-methoxyphenylborane complex (1312175-69-1)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ja2038485

Reference yield: 80.0%

1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 4-methoxyphenylborane complex (1312175-69-1) → C27H36BF3N2 (1338728-82-7)

Guidance literature:

With trityl tetrafluoroborate; phenol; In dichloromethane; at 20 ℃; for 0.0833333h; Inert atmosphere;

DOI:10.1055/s-0033-1338847

Reference yield:

1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 4-methoxyphenylborane complex (1312175-69-1) → ((H2C2N2(C6H3(CH(CH3)2)2)2C)BHC6H4OCH3)2

Guidance literature:

Multi-step reaction with 2 steps

1: di-tert-butyl peroxide / not given

2: benzene

With di-tert-butyl peroxide; In benzene;

DOI:10.1021/ja2038485

upstream raw materials:

4-methoxyphenylboronic acid

1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene

Downstream raw materials:

1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene-4-methoxyphenylborane radical

C₂₇H₃₆BF₃N₂

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