Allyl 3-O-benzyl-4,6-O-benzylidene-2-<2-(benzyloxycarbonyl)benzamido>-2-deoxy-α-D-allopyranoside

Base Information

Chemical Name:Allyl 3-O-benzyl-4,6-O-benzylidene-2-<2-(benzyloxycarbonyl)benzamido>-2-deoxy-α-D-allopyranoside
CAS No.:136773-80-3
Molecular Formula:C₃₈H₃₇NO₈
Molecular Weight:635.714
Hs Code.:

Synonyms:Allyl 3-O-benzyl-4,6-O-benzylidene-2-<2-(benzyloxycarbonyl)benzamido>-2-deoxy-α-D-allopyranoside

Suppliers and Price of Allyl 3-O-benzyl-4,6-O-benzylidene-2-<2-(benzyloxycarbonyl)benzamido>-2-deoxy-α-D-allopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Allyl 3-O-benzyl-4,6-O-benzylidene-2-<2-(benzyloxycarbonyl)benzamido>-2-deoxy-α-D-allopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Allyl 3-O-benzyl-4,6-O-benzylidene-2-<2-(benzyloxycarbonyl)benzamido>-2-deoxy-α-D-allopyranoside

There total 6 articles about Allyl 3-O-benzyl-4,6-O-benzylidene-2-<2-(benzyloxycarbonyl)benzamido>-2-deoxy-α-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 100-39-0
benzyl bromide

: 136845-45-9
Allyl 4,6-O-benzylidene-2-(2-carboxybenzamido)-2-deoxy-α-D-allopyranoside

: N-((2R,4aR,6S,7R,8S,8aS)-6-Allyloxy-8-benzyloxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-phthalamic acid

: 136773-80-3
Allyl 3-O-benzyl-4,6-O-benzylidene-2-<2-(benzyloxycarbonyl)benzamido>-2-deoxy-α-D-allopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 48h; Ambient temperature;
DOI:10.1039/c39910001099

Reference yield:

: 136773-79-0
Allyl 2-Amino-4,6-O-benzylidene-2-deoxy-α-D-allopyranoside

: 136773-80-3
Allyl 3-O-benzyl-4,6-O-benzylidene-2-<2-(benzyloxycarbonyl)benzamido>-2-deoxy-α-D-allopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Et₃N / methanol / 0.5 h / Ambient temperature

2: 44 percent / NaH / dimethylformamide / 24 h / Ambient temperature

With sodium hydride; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19920750505

Reference yield:

: 136845-44-8
Allyl 2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-allopyranoside

: 136773-80-3
Allyl 3-O-benzyl-4,6-O-benzylidene-2-<2-(benzyloxycarbonyl)benzamido>-2-deoxy-α-D-allopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / 1 N aq. NaOH / 144 h / Heating

2: 95 percent / Et₃N / methanol / 0.5 h / Ambient temperature

3: 44 percent / NaH / dimethylformamide / 24 h / Ambient temperature

With sodium hydroxide; sodium hydride; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19920750505