methyl 6-nitroheptanoate

Base Information

Chemical Name:methyl 6-nitroheptanoate
CAS No.:80594-94-1
Molecular Formula:C₈H₁₅NO₄
Molecular Weight:189.211
Hs Code.:

Synonyms:methyl 6-nitroheptanoate

Suppliers and Price of methyl 6-nitroheptanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 6-nitroheptanoate

Chemical Property:

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Technology Process of methyl 6-nitroheptanoate

There total 3 articles about methyl 6-nitroheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 4883-67-4
2-nitrocyclohexanone

: 74-88-4
methyl iodide

: 80594-87-2
2-methyl-2-nitrocyclohexan-1-one

: 13154-40-0
6-nitrohexanoic acid methyl ester

: 80594-94-1
methyl 6-nitroheptanoate

Guidance literature:: 2-nitrocyclohexanone; With tetra(n-butyl)ammonium hydroxide; In dichloromethane; water; for 0.166667h; Inert atmosphere;

methyl iodide; In dichloromethane; water; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1016/j.tet.2018.01.055

Reference yield:

: 4883-67-4
2-nitrocyclohexanone

: 80594-87-2
2-methyl-2-nitrocyclohexan-1-one

: 80594-94-1
methyl 6-nitroheptanoate

Guidance literature:: With tetra(n-butyl)ammonium hydroxide; 1.) methylene dichloride, 10 min, 2.) RT, 36 h;
DOI:10.1021/jo00346a006

Reference yield:

: 4883-67-4
2-nitrocyclohexanone

: 74-88-4
methyl iodide

: 80594-87-2
2-methyl-2-nitrocyclohexan-1-one

: 80594-94-1
methyl 6-nitroheptanoate

Guidance literature:: With tetra(n-butyl)ammonium hydroxide; Yield given. Multistep reaction; 1.) CH₂Cl₂, 10 min, 2.) RT, 36 h;
DOI:10.1021/jo00346a006