ethyl 2-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)oxazole-4-carboxylate

Base Information

Chemical Name:ethyl 2-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)oxazole-4-carboxylate
CAS No.:129149-87-7
Molecular Formula:C₃₂H₂₇NO₁₀
Molecular Weight:585.567
Hs Code.:

Synonyms:ethyl 2-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)oxazole-4-carboxylate

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Chemical Property of ethyl 2-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)oxazole-4-carboxylate

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Technology Process of ethyl 2-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)oxazole-4-carboxylate

There total 4 articles about ethyl 2-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)oxazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 129149-85-5
ethyl 5-amino-2-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)oxazole-4-carboxylate

: 129149-87-7
ethyl 2-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)oxazole-4-carboxylate

Guidance literature:: With hydrogenchloride; hypophosphorous acid; sodium nitrite; In tetrahydrofuran; at -20 ℃; for 4.25h;
DOI:10.1021/jm00172a027

Reference yield:

: 67560-74-1
3,4,6-tri-O-benzoyl-2,5-anhydro-D-allonic acid chloride

: 129149-87-7
ethyl 2-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)oxazole-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 21 percent / pyridine / 13 h / Ambient temperature

2: 56 percent / hydrogen chloride (gas) / acetone / 22 h / 4 °C

3: 60 percent / 50percent aq. hypophosphorous acid, hydrochloric acid, NaNO₂ / tetrahydrofuran / 4.25 h / -20 °C

With pyridine; hydrogenchloride; hypophosphorous acid; sodium nitrite; In tetrahydrofuran; acetone;
DOI:10.1021/jm00172a027

Reference yield:

: 129149-81-1,129149-82-2
ethyl 2-<(3',4',6'-tri-O-benzoyl-2',5'-anhydroallonyl)amino>-2-cyanoacetate

: 129149-87-7
ethyl 2-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)oxazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / hydrogen chloride (gas) / acetone / 22 h / 4 °C

2: 60 percent / 50percent aq. hypophosphorous acid, hydrochloric acid, NaNO₂ / tetrahydrofuran / 4.25 h / -20 °C

With hydrogenchloride; hypophosphorous acid; sodium nitrite; In tetrahydrofuran; acetone;
DOI:10.1021/jm00172a027