5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl 2-methyl-6-oxo-4-phenyl-1,4,5,6-tetrahydropyridine-3-carboxylate

Base Information

Chemical Name:5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl 2-methyl-6-oxo-4-phenyl-1,4,5,6-tetrahydropyridine-3-carboxylate
CAS No.:1313406-27-7
Molecular Formula:C₂₅H₂₀F₁₇NO₃
Molecular Weight:705.412
Hs Code.:

Synonyms:5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl 2-methyl-6-oxo-4-phenyl-1,4,5,6-tetrahydropyridine-3-carboxylate

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Chemical Property of 5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl 2-methyl-6-oxo-4-phenyl-1,4,5,6-tetrahydropyridine-3-carboxylate

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Technology Process of 5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl 2-methyl-6-oxo-4-phenyl-1,4,5,6-tetrahydropyridine-3-carboxylate

There total 1 articles about 5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl 2-methyl-6-oxo-4-phenyl-1,4,5,6-tetrahydropyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 2033-24-1
cycl-isopropylidene malonate

: 1313406-25-5
C₁₆H₁₃F₁₇O₃

: 100-52-7
benzaldehyde

: 1313406-27-7
5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl 2-methyl-6-oxo-4-phenyl-1,4,5,6-tetrahydropyridine-3-carboxylate

Guidance literature:: With ammonium acetate; In acetic acid; oil bath;
DOI:10.1016/j.jfluchem.2011.04.008

Reference yield:

: 1313406-27-7
5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl 2-methyl-6-oxo-4-phenyl-1,4,5,6-tetrahydropyridine-3-carboxylate

: 1313406-31-3
1-[3-(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyloxycarbonyl)-6-oxo-4-phenyl-1,4,5,6-tetrahydro-pyridin-2-ylmethyl]pyridinium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / chloroform / 0.5 h

2: acetone

With bromine; In chloroform; acetone;
DOI:10.1016/j.jfluchem.2011.04.008

Reference yield:

: 1313406-27-7
5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl 2-methyl-6-oxo-4-phenyl-1,4,5,6-tetrahydropyridine-3-carboxylate

: 1313406-33-5
1-[3-(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyloxycarbonyl)-6-oxo-4-phenyl-1,4,5,6-tetrahydro-pyridin-2-ylmethyl]-triphenylphosphonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / chloroform / 0.5 h

2: acetonitrile / 2 h / 40 °C

With bromine; In chloroform; acetonitrile;
DOI:10.1016/j.jfluchem.2011.04.008