Technology Process of C13H11N7O2S
There total 6 articles about C13H11N7O2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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Multi-step reaction with 5 steps
1.1: iron(III) chloride; sodium acetate / acetic acid / 0.5 h / 20 °C
2.1: sodium hydride / tetrahydrofuran; mineral oil / 5 - 20 °C / Inert atmosphere
2.2: 5 °C / Inert atmosphere
3.1: ethanol; sodium hydroxide / 20 °C / Reflux
4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere
5.1: trifluoroacetic acid / ethanol / 20 °C
With
iron(III) chloride; ethanol; sodium acetate; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; acetic acid; mineral oil;
DOI:10.1016/j.bmcl.2011.08.022
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ethanol; sodium hydroxide / 20 °C / Reflux
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C / Inert atmosphere
3: trifluoroacetic acid / ethanol / 20 °C
With
ethanol; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; sodium hydroxide;
In
ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.08.022
