5-dimethylamino-naphthalene-1-sulfonic acid (2-hydroxy-ethyl)-methyl-amide

Base Information

Chemical Name:5-dimethylamino-naphthalene-1-sulfonic acid (2-hydroxy-ethyl)-methyl-amide
CAS No.:41688-01-1
Molecular Formula:C₁₅H₂₀N₂O₃S
Molecular Weight:308.401
Hs Code.:

Synonyms:5-dimethylamino-naphthalene-1-sulfonic acid (2-hydroxy-ethyl)-methyl-amide

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Chemical Property of 5-dimethylamino-naphthalene-1-sulfonic acid (2-hydroxy-ethyl)-methyl-amide

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Technology Process of 5-dimethylamino-naphthalene-1-sulfonic acid (2-hydroxy-ethyl)-methyl-amide

There total 1 articles about 5-dimethylamino-naphthalene-1-sulfonic acid (2-hydroxy-ethyl)-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1064690-68-1
1-naphthylacetic acid (N-methyl-N-dansyl-2-amino)ethyl ester

: 86-87-3
naphth-1-yl acetic acid

: 41688-01-1
5-dimethylamino-naphthalene-1-sulfonic acid (2-hydroxy-ethyl)-methyl-amide

Guidance literature:: With sodium hydroxide; pig liver esterase; In phosphate buffer; acetonitrile; at 20 ℃; Enzyme kinetics;
DOI:10.1016/j.tet.2008.06.051

Reference yield: 87.0%

: 17261-28-8
ortho-diphenylphosphinobenzoic acid

: 41688-01-1
5-dimethylamino-naphthalene-1-sulfonic acid (2-hydroxy-ethyl)-methyl-amide

: 2-[5-(dimethylamino)-N-methylnaphthalene-1-sulfonamido]ethyl 2-(diphenylphosphino)benzoate

Guidance literature:: ortho-diphenylphosphinobenzoic acid; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 0.166667h;

5-dimethylamino-naphthalene-1-sulfonic acid (2-hydroxy-ethyl)-methyl-amide; at 20 ℃; Inert atmosphere;
DOI:10.1002/asia.201800503

Reference yield:

: 41688-01-1
5-dimethylamino-naphthalene-1-sulfonic acid (2-hydroxy-ethyl)-methyl-amide

: (4-{3-[tert-butoxycarbonyl-(2-methyl-4-o-tolylazo-phenyl)-amino]-propyl}-phenyl)-cyano-acetic acid 2-[(5-dimethylamino-naphthalene-1-sulfonyl)-methyl-amino]-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 96 percent / 4-dimethylaminopyridine; triethylamine; diisopropylcarbodiimide / tetrahydrofuran / 20 °C

2.1: NaH / toluene / 0.33 h / 20 °C

2.2: 77 percent / Pd(OAc)2; P(t-Bu)3 / toluene / 2.5 h / 100 - 105 °C

With dmap; sodium hydride; triethylamine; diisopropyl-carbodiimide; In tetrahydrofuran; toluene;
DOI:10.1021/ja0157402