Phosphoric acid (2R,3S,5R)-5-(6-amino-purin-9-yl)-2-methyl-tetrahydro-furan-3-yl ester 2-[(5-dimethylamino-naphthalene-1-sulfonyl)-methyl-amino]-ethyl ester 4-nitro-phenyl ester

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Chemical Name:Phosphoric acid (2R,3S,5R)-5-(6-amino-purin-9-yl)-2-methyl-tetrahydro-furan-3-yl ester 2-[(5-dimethylamino-naphthalene-1-sulfonyl)-methyl-amino]-ethyl ester 4-nitro-phenyl ester
CAS No.:171071-36-6
Molecular Formula:C₃₁H₃₅N₈O₉PS
Molecular Weight:726.707
Hs Code.:

Phosphoric acid (2R,3S,5R)-5-(6-amino-purin-9-yl)-2-methyl-tetrahydro-furan-3-yl ester 2-[(5-dimethylamino-naphthalene-1-sulfonyl)-methyl-amino]-ethyl ester 4-nitro-phenyl ester

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Chemical Property of Phosphoric acid (2R,3S,5R)-5-(6-amino-purin-9-yl)-2-methyl-tetrahydro-furan-3-yl ester 2-[(5-dimethylamino-naphthalene-1-sulfonyl)-methyl-amino]-ethyl ester 4-nitro-phenyl ester

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Technology Process of Phosphoric acid (2R,3S,5R)-5-(6-amino-purin-9-yl)-2-methyl-tetrahydro-furan-3-yl ester 2-[(5-dimethylamino-naphthalene-1-sulfonyl)-methyl-amino]-ethyl ester 4-nitro-phenyl ester

There total 4 articles about Phosphoric acid (2R,3S,5R)-5-(6-amino-purin-9-yl)-2-methyl-tetrahydro-furan-3-yl ester 2-[(5-dimethylamino-naphthalene-1-sulfonyl)-methyl-amino]-ethyl ester 4-nitro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 605-65-2
5-(dimethylamino)naphth-1-ylsulfonyl chloride

: 171071-36-6
Phosphoric acid (2R,3S,5R)-5-(6-amino-purin-9-yl)-2-methyl-tetrahydro-furan-3-yl ester 2-[(5-dimethylamino-naphthalene-1-sulfonyl)-methyl-amino]-ethyl ester 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / 2percent NaHCO₃ / acetone / Ambient temperature

2: 1.) t-BuMgCl, 2.) t-BuMgCl / 1.) THF, 15 deg C, 90 min, 2.) THF, room temperature, 4 h

With tert-butylmagnesium chloride; sodium hydrogencarbonate; In acetone;
DOI:10.1080/15257779508010705

Reference yield:

: 108906-82-7
(2S,3S,5R)-5-(6-Amino-purin-9-yl)-2-phenylsulfanylmethyl-tetrahydro-furan-3-ol

: 171071-36-6
Phosphoric acid (2R,3S,5R)-5-(6-amino-purin-9-yl)-2-methyl-tetrahydro-furan-3-yl ester 2-[(5-dimethylamino-naphthalene-1-sulfonyl)-methyl-amino]-ethyl ester 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / Raney Ni / methanol; propan-2-ol / 48 h / Heating

2: 1.) t-BuMgCl, 2.) t-BuMgCl / 1.) THF, 15 deg C, 90 min, 2.) THF, room temperature, 4 h

With tert-butylmagnesium chloride; nickel; In methanol; isopropyl alcohol;
DOI:10.1080/15257779508010705

Reference yield:

: 958-09-8,7005-15-4
2'-deoxy-D-adenosine

: 171071-36-6
Phosphoric acid (2R,3S,5R)-5-(6-amino-purin-9-yl)-2-methyl-tetrahydro-furan-3-yl ester 2-[(5-dimethylamino-naphthalene-1-sulfonyl)-methyl-amino]-ethyl ester 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / Bu₃P / pyridine / 12 h / Ambient temperature

2: 72 percent / Raney Ni / methanol; propan-2-ol / 48 h / Heating

3: 1.) t-BuMgCl, 2.) t-BuMgCl / 1.) THF, 15 deg C, 90 min, 2.) THF, room temperature, 4 h

With tributylphosphine; tert-butylmagnesium chloride; nickel; In pyridine; methanol; isopropyl alcohol;
DOI:10.1080/15257779508010705