(1R,2R,3R,4S,5S)-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane-1-ol

Base Information

Chemical Name:(1R,2R,3R,4S,5S)-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane-1-ol
CAS No.:1208102-24-2
Molecular Formula:C₃₆H₃₈O₆
Molecular Weight:566.694
Hs Code.:

Synonyms:(1R,2R,3R,4S,5S)-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane-1-ol

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Chemical Property of (1R,2R,3R,4S,5S)-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane-1-ol

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Technology Process of (1R,2R,3R,4S,5S)-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane-1-ol

There total 2 articles about (1R,2R,3R,4S,5S)-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1208102-29-7
(2R,3R,4R,5R)-5-benzoyloxy-3,4-dibenzyloxy-2-benzyloxymethyl-cycloheptanone

: 1208102-35-5
C₃₆H₃₈O₆

: 1208102-24-2
(1R,2R,3R,4S,5S)-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane-1-ol

Guidance literature:: With lithium tri-t-butoxyaluminum hydride; In diethyl ether; at -78 ℃; optical yield given as %de;
DOI:10.1039/b918576c

Reference yield:

: 1208102-23-1
C₄₄H₄₆O₇

: 1208102-24-2
(1R,2R,3R,4S,5S)-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane-1-ol

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; for 1h;
DOI:10.1039/b918576c

Reference yield: 76.0%

: 1208102-24-2
(1R,2R,3R,4S,5S)-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane-1-ol

: 1208102-25-3
(1R,2R,3R,4R,5R)-5-azido-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane

Guidance literature:: (1R,2R,3R,4S,5S)-1-benzoyloxy-2,3-dibenzyloxy-4-benzyloxymethyl-cycloheptane-1-ol; With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

With diphenyl phosphoryl azide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/b918576c