1-{(dimethylamino)methyl}-2-{(4-chlorophenyl)seleno}ferrocene

Base Information

Chemical Name:1-{(dimethylamino)methyl}-2-{(4-chlorophenyl)seleno}ferrocene
CAS No.:100113-88-0
Molecular Formula:C₁₉H₂₀ClFeNSe
Molecular Weight:432.634
Hs Code.:

Synonyms:1-{(dimethylamino)methyl}-2-{(4-chlorophenyl)seleno}ferrocene

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Chemical Property of 1-{(dimethylamino)methyl}-2-{(4-chlorophenyl)seleno}ferrocene

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Technology Process of 1-{(dimethylamino)methyl}-2-{(4-chlorophenyl)seleno}ferrocene

There total 1 articles about 1-{(dimethylamino)methyl}-2-{(4-chlorophenyl)seleno}ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1271-86-9
N,N-dimethylaminomethylferrocene

: 20541-49-5
bis(p-chlorophenyl) diselenide

: 100113-88-0
1-{(dimethylamino)methyl}-2-{(4-chlorophenyl)seleno}ferrocene

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; 2.7 M n-BuLi in hexane added over 0.5 h to CpFeC5H4CH2NMe2 in dry ether under Ar, stirred for 3 h at room temp., soln. of (C6H4Cl)2Se2 in ether added dropwise over 30 min at -78°C, stirred for 30 h, heated at reflux for 4 h, aq. NaHCO3 added; org. layer and ether exts. from aq. layer washed with ice water, dried over anhyd. Na2SO4, concd. in vac., chromd. (SiO2 column, hexane/C6H6/ether); elem. anal.;

Reference yield: 83.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 100113-88-0
1-{(dimethylamino)methyl}-2-{(4-chlorophenyl)seleno}ferrocene

: {1-{(dimethylamino)methyl}-2-(4-chlorophenylseleno)ferrocene}palladium(II) dichloride

Guidance literature:: In benzene; (PhCN)2PdCl2 and CpFe(C5H3(SeC6H4Cl)CH2NMe2) stirred in C6H6 at room temp. for 20 h; ppt. filtered, washed with C6H6, dried in vac., recrystd. from CH2Cl2/hexane; elem. anal.;