(R)-2-((R)-2-Acetoxy-2-phenyl-ethyl)-6-methoxy-piperidine-1-carboxylic acid methyl ester

Base Information

Chemical Name:(R)-2-((R)-2-Acetoxy-2-phenyl-ethyl)-6-methoxy-piperidine-1-carboxylic acid methyl ester
CAS No.:134040-05-4
Molecular Formula:C₁₈H₂₅NO₅
Molecular Weight:335.4
Hs Code.:

Synonyms:(R)-2-((R)-2-Acetoxy-2-phenyl-ethyl)-6-methoxy-piperidine-1-carboxylic acid methyl ester

Suppliers and Price of (R)-2-((R)-2-Acetoxy-2-phenyl-ethyl)-6-methoxy-piperidine-1-carboxylic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (R)-2-((R)-2-Acetoxy-2-phenyl-ethyl)-6-methoxy-piperidine-1-carboxylic acid methyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (R)-2-((R)-2-Acetoxy-2-phenyl-ethyl)-6-methoxy-piperidine-1-carboxylic acid methyl ester

There total 7 articles about (R)-2-((R)-2-Acetoxy-2-phenyl-ethyl)-6-methoxy-piperidine-1-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76469-99-3
1-(carbomethoxy)-2-phenacylpiperidine

: 134040-05-4
(R)-2-((R)-2-Acetoxy-2-phenyl-ethyl)-6-methoxy-piperidine-1-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Li(tBuO)3AlH / tetrahydrofuran / 4 h / Heating

2: 100 percent / pyridine / 15 h / Ambient temperature

3: 343 mg / Et₄NOTs / 0.17 h / anodic methoxylation

With pyridine; tetraethylammonium tosylate; lithium tri-t-butoxyaluminum hydride; In tetrahydrofuran;
DOI:10.1139/v91-034

Reference yield:

: 30800-90-9
1-phenyl-2-(piperidin-2-yl)ethan-1-one

: 134040-05-4
(R)-2-((R)-2-Acetoxy-2-phenyl-ethyl)-6-methoxy-piperidine-1-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / K₂CO₃ / H₂O / 15 h

2: Li(tBuO)3AlH / tetrahydrofuran / 4 h / Heating

3: 100 percent / pyridine / 15 h / Ambient temperature

4: 343 mg / Et₄NOTs / 0.17 h / anodic methoxylation

With pyridine; potassium carbonate; tetraethylammonium tosylate; lithium tri-t-butoxyaluminum hydride; In tetrahydrofuran; water;
DOI:10.1139/v91-034

Reference yield:

: 1415-36-7
(-)-norsedamine

: 134040-05-4
(2S,6R)-2-((S)-2-Acetoxy-2-phenyl-ethyl)-6-methoxy-piperidine-1-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / K₂CO₃ / H₂O / 4 h

2: pyridine / 15 h / Ambient temperature

3: Et₄NOTs / 0.17 h / anodic methoxylation

With pyridine; potassium carbonate; tetraethylammonium tosylate; In water;
DOI:10.1139/v91-034