furfuryl-2-(N-diphenylphosphino)methylamine

Base Information

Chemical Name:furfuryl-2-(N-diphenylphosphino)methylamine
CAS No.:586985-91-3
Molecular Formula:C₁₇H₁₆NOP
Molecular Weight:281.294
Hs Code.:

Synonyms:furfuryl-2-(N-diphenylphosphino)methylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of furfuryl-2-(N-diphenylphosphino)methylamine

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Technology Process of furfuryl-2-(N-diphenylphosphino)methylamine

There total 1 articles about furfuryl-2-(N-diphenylphosphino)methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.1%

: 617-89-0
furan-2-ylmethanamine

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 586985-91-3
furfuryl-2-(N-diphenylphosphino)methylamine

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 1h;
DOI:10.1002/aoc.1853

Reference yield: 94.1%

: 37366-09-9
dichloro(benzene)ruthenium(II) dimer

: 586985-91-3
furfuryl-2-(N-diphenylphosphino)methylamine

: 1357486-81-7
Ru(Ph2PNHCH2-C4H3O)(η-6-benzene)Cl2

Guidance literature:: In tetrahydrofuran; under Ar using Schlenk techniques; mixt. of org. ligand (1.02 mmol) and Ru complex (0.51 mmol) in THF stirred (room temp., 2 h); partially evapd.; Et2O added; ppt. filtered; dried (vac.); elem. anal.;
DOI:10.1016/j.poly.2012.05.009

Reference yield: 93.5%

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 586985-91-3
furfuryl-2-(N-diphenylphosphino)methylamine

: 1357486-80-6
[Ru(Ph2PNHCH2(C4H3O))(η6-p-cymene)Cl2]

Guidance literature:: In tetrahydrofuran; under Ar using Schlenk techniques; soln. of org. ligand (1.02 mmol) added to soln. of Ru complex (0.51 mmol); stirred (room temp., 1 h); filtered off; evapd. (vac.); solid washed with Et2O; dried (vac.); recrystd. from Et2O/CH2Cl2; elem. anal.;
DOI:10.1016/j.poly.2012.05.009