4,10,14-tribenzyl-12-methylene-4,10,14-triaza-1,7-dioxacyclohexadecane

Base Information

Chemical Name:4,10,14-tribenzyl-12-methylene-4,10,14-triaza-1,7-dioxacyclohexadecane
CAS No.:124243-39-6
Molecular Formula:C₃₃H₄₃N₃O₂
Molecular Weight:513.723
Hs Code.:

Synonyms:4,10,14-tribenzyl-12-methylene-4,10,14-triaza-1,7-dioxacyclohexadecane

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Chemical Property of 4,10,14-tribenzyl-12-methylene-4,10,14-triaza-1,7-dioxacyclohexadecane

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Technology Process of 4,10,14-tribenzyl-12-methylene-4,10,14-triaza-1,7-dioxacyclohexadecane

There total 5 articles about 4,10,14-tribenzyl-12-methylene-4,10,14-triaza-1,7-dioxacyclohexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1871-57-4
2-chloromethyl-3-chloroprop-1-ene

: 124243-49-8
Benzyl-bis-[2-(2-benzylamino-ethoxy)-ethyl]-amine

: 124243-39-6
4,10,14-tribenzyl-12-methylene-4,10,14-triaza-1,7-dioxacyclohexadecane

Guidance literature:: With sodium carbonate; sodium iodide; In acetonitrile; for 24h; Heating;
DOI:10.1021/jo00278a016

Reference yield:

: 91131-32-7
N-<2-2(-chloroethoxy)ethyl>benzamide

: 124243-39-6
4,10,14-tribenzyl-12-methylene-4,10,14-triaza-1,7-dioxacyclohexadecane

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / sodium carbonate, sodium iodide / acetonitrile / 48 h / Heating

2: lithium aluminum hydride / tetrahydrofuran / 24 h / Heating

3: 63 percent / sodium carbonate , sodium iodide / acetonitrile / 24 h / Heating

With lithium aluminium tetrahydride; sodium carbonate; sodium iodide; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00278a016

Reference yield:

: 124243-65-8
N-<2-(2-hydroxyethoxy)ethyl>benzamide

: 124243-39-6
4,10,14-tribenzyl-12-methylene-4,10,14-triaza-1,7-dioxacyclohexadecane

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / SOCl₂ / CHCl₃ / 1.) room temp., 1 h, 2.) reflux, 4 h

2: 55 percent / sodium carbonate, sodium iodide / acetonitrile / 48 h / Heating

3: lithium aluminum hydride / tetrahydrofuran / 24 h / Heating

4: 63 percent / sodium carbonate , sodium iodide / acetonitrile / 24 h / Heating

With lithium aluminium tetrahydride; thionyl chloride; sodium carbonate; sodium iodide; In tetrahydrofuran; chloroform; acetonitrile;
DOI:10.1021/jo00278a016