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BLOOM TECH Advanced API/Technology support 3-Chloro-2-(chloromethyl)prop-1-ene CAS 1871-57-4
Cas No: 1871-57-4
USD $ 5.0-5.0 / Gram 1 Gram 360 Kilogram/Month Shaanxi BLOOM TECH Co.,Ltd Contact Supplier
3-Chloro-2-chloromethyl-1-propene
Cas No: 1871-57-4
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Factory Supply 3-Chloro-2-Chloromethyl-Propene
Cas No: 1871-57-4
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Amadis Chemical offer CAS#1871-57-4;CAT#A813121
Cas No: 1871-57-4
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3-Chloro-2-chloromethyl-1-propene
Cas No: 1871-57-4
USD $ 1.0-1.0 / Kilogram 1 Kilogram 1000 Kilogram/Month Enke Pharma-tech Co.,Ltd. (Cangzhou, China ) Contact Supplier
3-Chloro-2-chloromethyl-1-propene / LIDE PHARMA- Factory supply / Best price
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C4H6Cl2 2-(CHLOROMETHYL)ALLYLTRICHLOROSILANE 1871-57-4
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3-Chloro-2-(chloromethyl)-1-propene
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1-Propene,3-chloro-2-(chloromethyl)-
Cas No: 1871-57-4
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1871-57-4 Usage

Chemical Properties

clear colorless to yellow liquid

Uses

3-Chloro-2-chloromethyl-1-propene can be used in the synthesis of 2,11-bis(methylidene)spermine, an inhibitor of spermine oxidase and branched side chains of conjugated polymers. It can also be used in the intermolecular [2+2] photocycloaddition during the total synthesis of (?)-grandisol.
InChI:InChI=1S/C4H6Cl2/c1-4(2-5)3-6/h1-3H2

1871-57-4 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Aldrich (C31104)  3-Chloro-2-chloromethyl-1-propene  99% 1871-57-4 C31104-10G 1,515.15CNY Detail
Aldrich (C31104)  3-Chloro-2-chloromethyl-1-propene  99% 1871-57-4 C31104-50G 4,197.96CNY Detail

1871-57-4SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 16, 2017

Revision Date: Aug 16, 2017

1.Identification

1.1 GHS Product identifier

Product name 3-chloro-2-(chloromethyl)prop-1-ene

1.2 Other means of identification

Product number -
Other names 3-Chloro-2-chloroMethyl-1-propene

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:1871-57-4 SDS

1871-57-4Synthetic route

3-chloro-2,2-bis(chloromethyl)propionic acid-1
17831-70-8

3-chloro-2,2-bis(chloromethyl)propionic acid-1

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

Conditions
ConditionsYield
at 205 - 215℃; Pyrolysis;99%
With quinoline
at 200 - 220℃; in presence of quinoline the pyrolysis begins at 100 deg C.; Yield given;
at 210℃; Yield given;
1,3-dichloro-2-chloromethylpropane
66703-69-3

1,3-dichloro-2-chloromethylpropane

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene 70 deg C, 24 h; 190 deg C;80%
5,5-dichloromethyl-2-thia-1,3-dioxane 2-oxide
2210-05-1

5,5-dichloromethyl-2-thia-1,3-dioxane 2-oxide

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

Conditions
ConditionsYield
at 500℃; under 1 Torr; Inert atmosphere; Pyrolysis;65%
2-(Hydroxymethyl)allyl alcohol
3513-81-3

2-(Hydroxymethyl)allyl alcohol

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

Conditions
ConditionsYield
With pyridine; thionyl chloride In dichloromethane for 3h; Reflux;32%
With pyridine; thionyl chloride; chloroform
2,2-bis(chloromethyl)aziridine

2,2-bis(chloromethyl)aziridine

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

Conditions
ConditionsYield
With hydrogenchloride; sodium nitrite In water at 5 - 50℃; for 5h; Large scale;29.1%
With hydrogenchloride; sodium nitrite at 20 - 50℃; Ring cleavage; elimination;85.0 g
quinoline
91-22-5

quinoline

3-chloro-2,2-bis(chloromethyl)propionic acid-1
17831-70-8

3-chloro-2,2-bis(chloromethyl)propionic acid-1

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

1,3-dichloro-2-methyl-propan-2-ol
597-32-0

1,3-dichloro-2-methyl-propan-2-ol

A

1,3-dichloro-2-methylpropene
3375-22-2

1,3-dichloro-2-methylpropene

B

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

Conditions
ConditionsYield
With sulfuric acid at 100℃; 1,3-dichloro-2-methyl-propene of uncertain stereochemical membership;
1,3-dichloro-2-methyl-propan-2-ol
597-32-0

1,3-dichloro-2-methyl-propan-2-ol

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

Conditions
ConditionsYield
With sulfuric acid at 100℃;
1,2,3-trichloro-2-methylpropane
1871-58-5

1,2,3-trichloro-2-methylpropane

A

1,3-dichloro-2-methylpropene
3375-22-2

1,3-dichloro-2-methylpropene

B

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

Conditions
ConditionsYield
at 450 - 460℃;
1-chloro-2,2-di(chloromethyl)-2-nitroethane
79437-10-8

1-chloro-2,2-di(chloromethyl)-2-nitroethane

A

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

B

1,3-dichloro-2-chloromethyl-1-propene
13245-65-3

1,3-dichloro-2-chloromethyl-1-propene

Conditions
ConditionsYield
With sodium amalgam
isobutene
115-11-7

isobutene

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

Conditions
ConditionsYield
beim Chlorieren;
With chlorine
3-Chloro-2-methylpropene
563-47-3

3-Chloro-2-methylpropene

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

Conditions
ConditionsYield
With tetrachloromethane at 20 - 30℃; beim Chlorieren;
With sodium carbonate beim Chlorieren;
3-Chloro-2-methylpropene
563-47-3

3-Chloro-2-methylpropene

A

1,3-dichloro-2-methylpropene
3375-22-2

1,3-dichloro-2-methylpropene

B

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

Conditions
ConditionsYield
With chlorine
(2-Chloro-1-chloromethyl-1-methyl-ethylselanyl)-benzene
81694-51-1

(2-Chloro-1-chloromethyl-1-methyl-ethylselanyl)-benzene

A

1,3-dichloro-2-methylpropene
3375-22-2

1,3-dichloro-2-methylpropene

B

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

Conditions
ConditionsYield
With 3-chloro-benzenecarboperoxoic acid In pyridine; dichloromethane 1.) -70 degC 2 h, 2.) R.T. overnight; Yield given;
isobutene
115-11-7

isobutene

A

2-methylprop-1-enyl chloride
513-37-1

2-methylprop-1-enyl chloride

B

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

C

1,2-dichloro-2-methylpropane
594-37-6

1,2-dichloro-2-methylpropane

D

(E)-1,3-Dichloro-2-methyl-1-propene
35329-41-0

(E)-1,3-Dichloro-2-methyl-1-propene

E

(Z)-1,3-Dichloro-2-methyl-1-propene
35329-40-9

(Z)-1,3-Dichloro-2-methyl-1-propene

F

3-Chloro-2-methylpropene
563-47-3

3-Chloro-2-methylpropene

Conditions
ConditionsYield
With chlorine at 40 - 70℃; Product distribution; various conc.; further products;
3-Chloro-2-methylpropene
563-47-3

3-Chloro-2-methylpropene

A

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

B

(E)-1,3-Dichloro-2-methyl-1-propene
35329-41-0

(E)-1,3-Dichloro-2-methyl-1-propene

C

(Z)-1,3-Dichloro-2-methyl-1-propene
35329-40-9

(Z)-1,3-Dichloro-2-methyl-1-propene

Conditions
ConditionsYield
With chlorine monofluoride In chloroform in the dark; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
3-Chloro-2-methylpropene
563-47-3

3-Chloro-2-methylpropene

A

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

B

1,2,3-trichloro-2-methylpropane
1871-58-5

1,2,3-trichloro-2-methylpropane

C

(E)-1,3-Dichloro-2-methyl-1-propene
35329-41-0

(E)-1,3-Dichloro-2-methyl-1-propene

D

(Z)-1,3-Dichloro-2-methyl-1-propene
35329-40-9

(Z)-1,3-Dichloro-2-methyl-1-propene

Conditions
ConditionsYield
With oxygen; phosphorus trichloride at 30℃;
tetrachloromethane
56-23-5

tetrachloromethane

chlorine
7782-50-5

chlorine

3-Chloro-2-methylpropene
563-47-3

3-Chloro-2-methylpropene

A

1,3-dichloro-2-methylpropene
3375-22-2

1,3-dichloro-2-methylpropene

B

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

C

1,2,3-trichloro-2-methylpropane
1871-58-5

1,2,3-trichloro-2-methylpropane

Conditions
ConditionsYield
at 20 - 30℃;
1,1-bis-chloromethyl-ethanediyl sulfite

1,1-bis-chloromethyl-ethanediyl sulfite

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

Conditions
ConditionsYield
With quartz at 500℃;
3-Chloro-2-methylpropene
563-47-3

3-Chloro-2-methylpropene

A

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

B

1ξ,3-dichloro-2-methyl-propene and 1,2,3-trichloro-2-methyl-propane

1ξ,3-dichloro-2-methyl-propene and 1,2,3-trichloro-2-methyl-propane

Conditions
ConditionsYield
With chlorine
2-methylprop-1-enyl chloride
513-37-1

2-methylprop-1-enyl chloride

chlorine
7782-50-5

chlorine

A

1,3-dichloro-2-methylpropene
3375-22-2

1,3-dichloro-2-methylpropene

B

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

C

1,1,2-trichloro-2-methylpropane
29559-52-2

1,1,2-trichloro-2-methylpropane

D

1,1,2,3-Tetrachlor-2-methylpropan
18963-01-4

1,1,2,3-Tetrachlor-2-methylpropan

Conditions
ConditionsYield
unter Lichtausschluss;Produkt 5:3,3-Dichlor-2-methyl-propen;
1-chloro-2,2-di(chloromethyl)-2-nitroethane
79437-10-8

1-chloro-2,2-di(chloromethyl)-2-nitroethane

sodium amalgam

sodium amalgam

A

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

B

1,3-dichloro-2-chloromethyl-1-propene
13245-65-3

1,3-dichloro-2-chloromethyl-1-propene

2-methylprop-1-enyl chloride
513-37-1

2-methylprop-1-enyl chloride

A

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

B

below/under light-exclusion

below/under light-exclusion

Conditions
ConditionsYield
With chlorine
5,5-dichloromethyl-2-thia-1,3-dioxane 2-oxide
2210-05-1

5,5-dichloromethyl-2-thia-1,3-dioxane 2-oxide

A

formaldehyd
50-00-0

formaldehyd

B

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

C

sulfur dioxide

sulfur dioxide

Conditions
ConditionsYield
at 500℃; beim Leiten ueber Quarz;
1,2,3-trichloro-2-methylpropane
1871-58-5

1,2,3-trichloro-2-methylpropane

A

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

B

trans-1.3-dichloro-2-methyl-propene-(1)

trans-1.3-dichloro-2-methyl-propene-(1)

C

cis-1.3-dichloro-2-methyl-propene-(1)

cis-1.3-dichloro-2-methyl-propene-(1)

Conditions
ConditionsYield
at 450 - 460℃;
sodium benzoate
532-32-1

sodium benzoate

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

1,3-dibenzoyl-(2-methylidene)-1,3-propanediol
39185-03-0

1,3-dibenzoyl-(2-methylidene)-1,3-propanediol

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 80℃; for 12h;99%
In N,N-dimethyl-formamide for 4h; Heating;73%
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol
100-79-8

(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

C16H28O6
1206187-88-3

C16H28O6

Conditions
ConditionsYield
Stage #1: (R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol With 15-crown-5; sodium hydride In tetrahydrofuran; mineral oil at 40℃; Inert atmosphere;
Stage #2: 2-chloromethyl-3-chloroprop-1-ene With 18-crown-6 ether; potassium iodide In tetrahydrofuran; mineral oil Inert atmosphere; Reflux;
99%
Stage #1: (R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol With 15-crown-5; sodium hydride In tetrahydrofuran at 50℃; for 1h;
Stage #2: 2-chloromethyl-3-chloroprop-1-ene With 18-crown-6 ether; potassium iodide In tetrahydrofuran at 80℃; for 12h;
56%
Stage #1: (R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol With 15-crown-5; sodium hydride In tetrahydrofuran; mineral oil at 40℃; Inert atmosphere;
Stage #2: 2-chloromethyl-3-chloroprop-1-ene With 18-crown-6 ether; potassium iodide In tetrahydrofuran; mineral oil Inert atmosphere; Reflux;
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

methylphenylphosphine
6372-48-1

methylphenylphosphine

(2-methylenepropane-1,3-diyl)bis(methylphenylphosphine sulfide)

(2-methylenepropane-1,3-diyl)bis(methylphenylphosphine sulfide)

Conditions
ConditionsYield
Stage #1: 2-chloromethyl-3-chloroprop-1-ene; methylphenylphosphine With [((R)-MeO-BiPHEP)(1,2-bis(dimethylphosphino)ethane)Ru(H)][BPh4]; sodium tert-pentoxide In tetrahydrofuran at 23℃; for 1.5h; Inert atmosphere;
Stage #2: With borane-THF In tetrahydrofuran at 23℃; for 0.5h; Inert atmosphere; enantioselective reaction;
99%
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

1-Hexadecanol
36653-82-4

1-Hexadecanol

C36H72O2

C36H72O2

Conditions
ConditionsYield
With 15-crown-5; sodium hydride In tetrahydrofuran Reflux;99%
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

propargyl alcohol
107-19-7

propargyl alcohol

5-methylenenona-2,7-diyne-1,9-diol

5-methylenenona-2,7-diyne-1,9-diol

Conditions
ConditionsYield
With copper(l) iodide; potassium carbonate; sodium iodide In acetone for 17h; Reflux;99%
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

benzyl alcohol
100-51-6

benzyl alcohol

2-methylenepropane-1,3-bisbenzyl ether
27441-79-8

2-methylenepropane-1,3-bisbenzyl ether

Conditions
ConditionsYield
Stage #1: 2-chloromethyl-3-chloroprop-1-ene; benzyl alcohol With sodium hydride In tetrahydrofuran for 0.5h; Cooling with ice;
Stage #2: With 15-crown-5 In tetrahydrofuran for 14h; Reflux;
98%
Stage #1: benzyl alcohol With sodium hydride In N,N-dimethyl-formamide at 20℃; for 1h;
Stage #2: 2-chloromethyl-3-chloroprop-1-ene In N,N-dimethyl-formamide at 20℃; Further stages.;
97%
With sodium hydride In N,N-dimethyl-formamide at 20℃; for 12h;88%
With sodium hydride 1.) THF, 2.) a) room temperature, overnight, b) reflux, 5 h; Yield given. Multistep reaction;
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

1,5-bis(carboxyethyl)glycoluril
161146-03-8

1,5-bis(carboxyethyl)glycoluril

6-Methylene-1,4-dioxo-hexahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-2a,7b-dicarboxylic acid diethyl ester

6-Methylene-1,4-dioxo-hexahydro-2,3,4a,7a-tetraaza-cyclopenta[cd]indene-2a,7b-dicarboxylic acid diethyl ester

Conditions
ConditionsYield
With potassium tert-butylate In dimethyl sulfoxide98%
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

N,N-methylenediacetamide
3852-14-0

N,N-methylenediacetamide

5-exomethylene-1,3-diacetyl-1,3-diazacyclohexane
261508-08-1

5-exomethylene-1,3-diacetyl-1,3-diazacyclohexane

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran for 72h; Alkylation; Thermolysis;98%
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

1-Decanol
112-30-1

1-Decanol

1-(2-((decyloxy)methyl)allyloxy)decane
1259928-12-5

1-(2-((decyloxy)methyl)allyloxy)decane

Conditions
ConditionsYield
With 15-crown-5; sodium hydride In tetrahydrofuran for 20.25h; Reflux;98%
With sodium hydride In tetrahydrofuran at 20℃; Inert atmosphere;74%
With 15-crown-5; sodium hydride In tetrahydrofuran Reflux;
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

methyl 4,6-O-benzylidene-α-D-galactopyranoside
64552-06-3

methyl 4,6-O-benzylidene-α-D-galactopyranoside

methyl 4,6-O-(S)-benzylidene-2,3-O-(2-methylidene-1,3-propylene)-α-D-galactopyranoside
1263386-75-9

methyl 4,6-O-(S)-benzylidene-2,3-O-(2-methylidene-1,3-propylene)-α-D-galactopyranoside

Conditions
ConditionsYield
With 18-crown-6 ether; potassium hydroxide In tetrahydrofuran at 5 - 20℃;98%
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

C28H58O3

C28H58O3

C60H120O6

C60H120O6

Conditions
ConditionsYield
With 15-crown-5; sodium hydride In tetrahydrofuran Reflux;98%
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

n-eicosanol
629-96-9

n-eicosanol

C44H88O2

C44H88O2

Conditions
ConditionsYield
With 15-crown-5; sodium hydride In tetrahydrofuran Reflux;98%
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

para-tert-butylphenol
98-54-4

para-tert-butylphenol

C24H32O2
206653-69-2

C24H32O2

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide97%
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

(Nk-)4[G-3]-ol
245071-36-7

(Nk-)4[G-3]-ol

(Nk-)4[G-4]-methylallyl chloride
268567-74-4

(Nk-)4[G-4]-methylallyl chloride

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran97%
3-cyclohexyl-2-(2-hydroxy-phenyl)-1H-indole-6-carboxylic acid methyl ester
863578-50-1

3-cyclohexyl-2-(2-hydroxy-phenyl)-1H-indole-6-carboxylic acid methyl ester

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

methyl 14-cyclohexyl-7-methylene-7,8-dihydro-6H-indolo[1,2-e][1,5]benzoxazocine-11-carboxylate
886042-33-7

methyl 14-cyclohexyl-7-methylene-7,8-dihydro-6H-indolo[1,2-e][1,5]benzoxazocine-11-carboxylate

Conditions
ConditionsYield
Stage #1: 3-cyclohexyl-2-(2-hydroxy-phenyl)-1H-indole-6-carboxylic acid methyl ester With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 0.5h;
Stage #2: 2-chloromethyl-3-chloroprop-1-ene In N,N-dimethyl-formamide at 20℃;
97%
Stage #1: 3-cyclohexyl-2-(2-hydroxy-phenyl)-1H-indole-6-carboxylic acid methyl ester With sodium hydride In N,N-dimethyl-formamide for 0.5h;
Stage #2: 2-chloromethyl-3-chloroprop-1-ene In N,N-dimethyl-formamide at 20℃; for 1h;
70%
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

1,5-anhydro-4,6-O-(R)-benzylidene-D-glucitol
65391-44-8

1,5-anhydro-4,6-O-(R)-benzylidene-D-glucitol

1,5-anhydro-4,6-O-(R)-benzylidene-2,3-O-(2-methylidene-1,3-propylene)-D-glucitol
1263386-76-0

1,5-anhydro-4,6-O-(R)-benzylidene-2,3-O-(2-methylidene-1,3-propylene)-D-glucitol

Conditions
ConditionsYield
With 18-crown-6 ether; potassium hydroxide In tetrahydrofuran at 5 - 20℃;97%
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

methyl 4,6-O-(S)-benzylidene-β-D-galactopyranoside
71117-36-7

methyl 4,6-O-(S)-benzylidene-β-D-galactopyranoside

methyl 4,6-O-(S)-benzylidene-2,3-O-(2-methylidene-1,3-propylene)-β-D-galactopyranoside
1263386-73-7

methyl 4,6-O-(S)-benzylidene-2,3-O-(2-methylidene-1,3-propylene)-β-D-galactopyranoside

Conditions
ConditionsYield
With 18-crown-6 ether; potassium hydroxide In tetrahydrofuran at 5 - 20℃;97%
1-octadecanol
112-92-5

1-octadecanol

2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

1-(2-Octadecyloxymethyl-allyloxy)-octadecane

1-(2-Octadecyloxymethyl-allyloxy)-octadecane

Conditions
ConditionsYield
With 15-crown-5; sodium hydride In tetrahydrofuran Reflux;97%
2-chloromethyl-3-chloroprop-1-ene
1871-57-4

2-chloromethyl-3-chloroprop-1-ene

sodium thiomethoxide
5188-07-8

sodium thiomethoxide

3-methylsulfanyl-2-methylsulfanylmethylprop-1-ene
96694-05-2

3-methylsulfanyl-2-methylsulfanylmethylprop-1-ene

Conditions
ConditionsYield
With cetyltributylphosphonium bromide In water for 6h; Ambient temperature;96%
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