tert-butyl {3-[2-(6-methyl-2-oxo-7-oxabicyclo[4.1.0]hept-1-yl)ethyl]phenyl}carbamate

Base Information

Chemical Name:tert-butyl {3-[2-(6-methyl-2-oxo-7-oxabicyclo[4.1.0]hept-1-yl)ethyl]phenyl}carbamate
CAS No.:1338951-50-0
Molecular Formula:C₂₀H₂₇NO₄
Molecular Weight:345.439
Hs Code.:

Synonyms:tert-butyl {3-[2-(6-methyl-2-oxo-7-oxabicyclo[4.1.0]hept-1-yl)ethyl]phenyl}carbamate

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Chemical Property of tert-butyl {3-[2-(6-methyl-2-oxo-7-oxabicyclo[4.1.0]hept-1-yl)ethyl]phenyl}carbamate

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Technology Process of tert-butyl {3-[2-(6-methyl-2-oxo-7-oxabicyclo[4.1.0]hept-1-yl)ethyl]phenyl}carbamate

There total 4 articles about tert-butyl {3-[2-(6-methyl-2-oxo-7-oxabicyclo[4.1.0]hept-1-yl)ethyl]phenyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338951-78-2
tert-butyl {3-[2-(2-methyl-6-oxocyclohex-1-en-1-yl)ethyl]phenyl}carbamate

: 1338951-50-0
tert-butyl {3-[2-(6-methyl-2-oxo-7-oxabicyclo[4.1.0]hept-1-yl)ethyl]phenyl}carbamate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1016/j.tet.2011.08.050

Reference yield:

: 1338951-80-6
C₁₉H₂₅NO₄

: 1338951-50-0
tert-butyl {3-[2-(6-methyl-2-oxo-7-oxabicyclo[4.1.0]hept-1-yl)ethyl]phenyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: chloro-trimethyl-silane / 16 h / 20 °C / Inert atmosphere

2: diethyl ether / 2 h / 20 °C / Inert atmosphere

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 h / 20 °C / Inert atmosphere

With chloro-trimethyl-silane; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;
DOI:10.1016/j.tet.2011.08.050

Reference yield:

: 1227745-54-1
tert-butyl {3-[2-(2-hydroxy-6-oxocyclohex-1-en-1-yl)-3-oxoethyl]phenyl}carbamate

: 1338951-50-0
tert-butyl {3-[2-(6-methyl-2-oxo-7-oxabicyclo[4.1.0]hept-1-yl)ethyl]phenyl}carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; sodium cyanoborohydride / tetrahydrofuran; water / 0.5 h / 0 - 5 °C / Inert atmosphere

2: chloro-trimethyl-silane / 16 h / 20 °C / Inert atmosphere

3: diethyl ether / 2 h / 20 °C / Inert atmosphere

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 h / 20 °C / Inert atmosphere

With hydrogenchloride; chloro-trimethyl-silane; sodium cyanoborohydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1016/j.tet.2011.08.050