tert-butyl {3-[2-(2-hydroxy-6-oxocyclohex-1-en-1-yl)-3-oxoethyl]phenyl}carbamate

Base Information

Chemical Name:tert-butyl {3-[2-(2-hydroxy-6-oxocyclohex-1-en-1-yl)-3-oxoethyl]phenyl}carbamate
CAS No.:1227745-54-1
Molecular Formula:C₁₉H₂₃NO₅
Molecular Weight:345.395
Hs Code.:

Synonyms:tert-butyl {3-[2-(2-hydroxy-6-oxocyclohex-1-en-1-yl)-3-oxoethyl]phenyl}carbamate

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Chemical Property of tert-butyl {3-[2-(2-hydroxy-6-oxocyclohex-1-en-1-yl)-3-oxoethyl]phenyl}carbamate

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Technology Process of tert-butyl {3-[2-(2-hydroxy-6-oxocyclohex-1-en-1-yl)-3-oxoethyl]phenyl}carbamate

There total 1 articles about tert-butyl {3-[2-(2-hydroxy-6-oxocyclohex-1-en-1-yl)-3-oxoethyl]phenyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 504-02-9
1,3-cylohexanedione

: 123036-51-1
2-(3-((tert-butoxycarbonyl)amino)phenyl)acetic acid

: 1227745-54-1
tert-butyl {3-[2-(2-hydroxy-6-oxocyclohex-1-en-1-yl)-3-oxoethyl]phenyl}carbamate

Guidance literature:: With dmap; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 14h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.02.111

Reference yield: 81.0%

: 1227745-54-1
tert-butyl {3-[2-(2-hydroxy-6-oxocyclohex-1-en-1-yl)-3-oxoethyl]phenyl}carbamate

: 1338951-80-6
C₁₉H₂₅NO₄

Guidance literature:: With hydrogenchloride; sodium cyanoborohydride; In tetrahydrofuran; water; at 0 - 5 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tet.2011.08.050

Reference yield:

: 1227745-54-1
tert-butyl {3-[2-(2-hydroxy-6-oxocyclohex-1-en-1-yl)-3-oxoethyl]phenyl}carbamate

: 1338951-50-0
tert-butyl {3-[2-(6-methyl-2-oxo-7-oxabicyclo[4.1.0]hept-1-yl)ethyl]phenyl}carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; sodium cyanoborohydride / tetrahydrofuran; water / 0.5 h / 0 - 5 °C / Inert atmosphere

2: chloro-trimethyl-silane / 16 h / 20 °C / Inert atmosphere

3: diethyl ether / 2 h / 20 °C / Inert atmosphere

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 h / 20 °C / Inert atmosphere

With hydrogenchloride; chloro-trimethyl-silane; sodium cyanoborohydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1016/j.tet.2011.08.050