(Z)-ethyl 2-oxopropyl phenyldithioimidocarbonate

Base Information

• Chemical Name: (Z)-ethyl 2-oxopropyl phenyldithioimidocarbonate
• CAS No.: 1025476-25-8
• Molecular Formula: C₁₂H₁₅NOS₂
• Molecular Weight: 253.389

Synonyms:(Z)-ethyl 2-oxopropyl phenyldithioimidocarbonate

Chemical Property of (Z)-ethyl 2-oxopropyl phenyldithioimidocarbonate

Chemical Property:

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Technology Process of (Z)-ethyl 2-oxopropyl phenyldithioimidocarbonate

There total 1 articles about (Z)-ethyl 2-oxopropyl phenyldithioimidocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenyldithiocarbamic acid ethyl ester (13037-20-2) + 1-bromoacetone (598-31-2) → (Z)-ethyl 2-oxopropyl phenyldithioimidocarbonate (1025476-25-8)

Guidance literature:

With triethylamine; In acetone; at 20 ℃; for 0.5h;

DOI:10.1016/j.tetlet.2008.02.103

Reference yield: 67.0%

(Z)-ethyl 2-oxopropyl phenyldithioimidocarbonate (1025476-25-8) → rac-N-[(2Z)-5-methyl-1,3-oxathiolan-2-ylidene]aniline (101835-24-9)

Guidance literature:

With potassium hydroxide; sodium tetrahydroborate; In methanol; at 0 - 60 ℃; for 5.5h;

DOI:10.1016/j.tetlet.2008.02.103

Reference yield:

(Z)-ethyl 2-oxopropyl phenyldithioimidocarbonate (1025476-25-8) → (Z)-ethyl 2-hydroxypropyl phenyldithioimidocarbonate (1025476-74-7)

Guidance literature:

With sodium tetrahydroborate; In methanol;

DOI:10.1016/j.tetlet.2008.02.103

upstream raw materials:

phenyldithiocarbamic acid ethyl ester

1-bromoacetone

Downstream raw materials:

(Z)-ethyl 2-hydroxypropyl phenyldithioimidocarbonate

rac-N-[(2Z)-5-methyl-1,3-oxathiolan-2-ylidene]aniline

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