(E)-2-((2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-yl)amino)acetamide

Base Information

Chemical Name:(E)-2-((2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-yl)amino)acetamide
CAS No.:1353547-79-1
Molecular Formula:C₂₀H₂₅N₃O₇S
Molecular Weight:451.5
Hs Code.:

Synonyms:(E)-2-((2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-yl)amino)acetamide

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Chemical Property of (E)-2-((2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-yl)amino)acetamide

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Technology Process of (E)-2-((2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-yl)amino)acetamide

There total 11 articles about (E)-2-((2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-yl)amino)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1353547-77-9
(E)-2-((2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-yl)amino)acetic acid

: 1353547-79-1
(E)-2-((2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-yl)amino)acetamide

Guidance literature:: With ammonia; In methanol; water; at 60 ℃;
DOI:10.1021/jm4019614

Reference yield: 26.0%

: 1353547-76-8
(E)-ethyl 2-((2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-yl)amino)acetate

: 1353547-79-1
(E)-2-((2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-yl)amino)acetamide

Guidance literature:: With ammonia; In methanol; water; at 60 ℃; for 4h;

Reference yield:

: 23056-40-8
2-chloro-5-methyl-3-nitro-pyridine

: 1353547-79-1
(E)-2-((2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)pyridin-3-yl)amino)acetamide

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium / 4 h / Reflux; Inert atmosphere

2.1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 48 h / Inert atmosphere; Reflux

3.1: sodium carbonate / methanol / 1 h / 20 °C

4.1: dihydrogen peroxide; acetic acid / 6 h / 60 °C

5.1: water; sodium carbonate / methanol / 4 h / 20 °C

5.2: pH 2

6.1: piperidine; pyridine / 3 h / Inert atmosphere; Reflux

7.1: acetic acid; iron / methanol / 2 h / 50 °C / Inert atmosphere

8.1: potassium carbonate / N,N-dimethyl-formamide / 60 °C

9.1: ammonia / water; methanol / 4 h / 60 °C

With piperidine; pyridine; N-Bromosuccinimide; ammonia; water; dihydrogen peroxide; sodium; iron; sodium carbonate; potassium carbonate; acetic acid; dibenzoyl peroxide; In methanol; tetrachloromethane; water; N,N-dimethyl-formamide;