C₃₃H₄₅N₇O₁₇S

Base Information

• Chemical Name: C₃₃H₄₅N₇O₁₇S
• CAS No.: 1610414-00-0
• Molecular Formula: C₃₃H₄₅N₇O₁₇S
• Molecular Weight: 843.823
• Mol file: 1610414-00-0.mol

Synonyms:C₃₃H₄₅N₇O₁₇S

Chemical Property of C₃₃H₄₅N₇O₁₇S

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₃H₄₅N₇O₁₇S

There total 11 articles about C₃₃H₄₅N₇O₁₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

C34H54N4O10 (1610413-97-2) + C73H71ClN3O11PolS → C33H45N7O17S (1610414-00-0)

Guidance literature:

C₇₃H₇₁ClN₃O₁₁PolS; With piperidine; In N,N-dimethyl-formamide; isopropyl alcohol; at 20 ℃; not specified Inert atmosphere;

C₃₄H₅₄N₄O₁₀; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; for 1h; not specified Inert atmosphere;

With chlorotriisopropylsilane; trifluoroacetic acid; D,L-dithiothreitol; In water; not specified

Reference yield: 43.0%

H-cys(4-methoxytrityl)-2-chlorotrityl-resin + C34H54N4O10 (1610413-97-2) + Fmoc-(tBu)Asp-OH (71989-14-5) → C33H45N7O17S (1610414-00-0)

Guidance literature:

H-cys(4-methoxytrityl)-2-chlorotrityl-resin; Fmoc-(tBu)Asp-OH; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; not specified Inert atmosphere;

With piperidine; In N,N-dimethyl-formamide; not specified Inert atmosphere;

C₃₄H₅₄N₄O₁₀; Fmoc-(tBu)Asp-OH; Further stages;

Reference yield:

C22H20NO2PolS + C31H48N4O11 (1610413-98-3) + Fmoc-(tBu)Asp-OH (71989-14-5) + N-(9-fluorenylmethyloxycarbonyl)-4-(aminomethyl)phenylacetic acid (176504-01-1) → C33H45N7O17S (1610414-00-0)

Guidance literature:

C₂₂H₂₀NO₂PolS; Fmoc-(tBu)Asp-OH; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; not specified

With piperidine; In N,N-dimethyl-formamide; not specified

C₃₁H₄₈N₄O₁₁; Fmoc-(tBu)Asp-OH; N-(9-fluorenylmethyloxycarbonyl)-4-(aminomethyl)phenylacetic acid; Further stages;

upstream raw materials:

2-(4-(((tert-butoxycarbonyl)amino)methyl)phenyl)acetic acid

C₃₁H₄₈N₄O₁₁

2-(4-(aminomethyl)phenyl)acetic acid

C₃₄H₅₄N₄O₁₀