(2S,4S,5S,7S)-N-[4-azido-5-hydroxy-2,7-diisopropyl-octanedioic acid 8-butylamide]-1-[2-(3-methoxypropoxy)-benzyl]amide

Base Information

• Chemical Name: (2S,4S,5S,7S)-N-[4-azido-5-hydroxy-2,7-diisopropyl-octanedioic acid 8-butylamide]-1-[2-(3-methoxypropoxy)-benzyl]amide
• CAS No.: 179995-12-1
• Molecular Formula: C₂₉H₄₉N₅O₅
• Molecular Weight: 547.739

Synonyms:(2S,4S,5S,7S)-N-[4-azido-5-hydroxy-2,7-diisopropyl-octanedioic acid 8-butylamide]-1-[2-(3-methoxypropoxy)-benzyl]amide

Chemical Property of (2S,4S,5S,7S)-N-[4-azido-5-hydroxy-2,7-diisopropyl-octanedioic acid 8-butylamide]-1-[2-(3-methoxypropoxy)-benzyl]amide

Chemical Property:

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Technology Process of (2S,4S,5S,7S)-N-[4-azido-5-hydroxy-2,7-diisopropyl-octanedioic acid 8-butylamide]-1-[2-(3-methoxypropoxy)-benzyl]amide

There total 1 articles about (2S,4S,5S,7S)-N-[4-azido-5-hydroxy-2,7-diisopropyl-octanedioic acid 8-butylamide]-1-[2-(3-methoxypropoxy)-benzyl]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2S,2'S,2S,4S)-2-[2'-azido-2'-(4-isopropyl-5-oxo-tetrahydrofuran-2-yl)-ethyl]-N-[2-(3-methoxypropoxy)-benzyl]-3-methylbutyric acid amide (179995-08-5) + N-butylamine (109-73-9,85404-21-3) → (2S,4S,5S,7S)-N-[4-azido-5-hydroxy-2,7-diisopropyl-octanedioic acid 8-butylamide]-1-[2-(3-methoxypropoxy)-benzyl]amide (179995-12-1)

Guidance literature:

at 50 - 55 ℃; for 16h;

Reference yield:

(2S,4S,5S,7S)-N-[4-azido-5-hydroxy-2,7-diisopropyl-octanedioic acid 8-butylamide]-1-[2-(3-methoxypropoxy)-benzyl]amide (179995-12-1) → (2S,4S,5S,7S)-4-amino-5-hydroxy-2,7-diisopropyl-octanedioic acid 8-butylamide 1-[2-(3-methoxypropoxy)-benzyl]amide hydrochloride (179995-16-5)

Guidance literature:

With hydrogenchloride; hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 4h; pH=6;

upstream raw materials:

(2S,2'S,2S,4S)-2-[2'-azido-2'-(4-isopropyl-5-oxo-tetrahydrofuran-2-yl)-ethyl]-N-[2-(3-methoxypropoxy)-benzyl]-3-methylbutyric acid amide

N-butylamine

Downstream raw materials:

(2S,4S,5S,7S)-4-amino-5-hydroxy-2,7-diisopropyl-octanedioic acid 8-butylamide 1-[2-(3-methoxypropoxy)-benzyl]amide hydrochloride

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