4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]-2-methyl-benzamide

Base Information

Chemical Name:4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]-2-methyl-benzamide
CAS No.:1427274-94-9
Molecular Formula:C₁₈H₁₃Cl₂F₃N₂OS
Molecular Weight:433.281
Hs Code.:

Synonyms:4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]-2-methyl-benzamide

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Chemical Property of 4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]-2-methyl-benzamide

Chemical Property:

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Technology Process of 4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]-2-methyl-benzamide

There total 6 articles about 4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]-2-methyl-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427274-93-8
C₁₈H₁₁Cl₃F₃NOS

: 1427274-94-9
4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]-2-methyl-benzamide

Guidance literature:: With ammonium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 2h;

Reference yield:

: 1427274-51-8
4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]-2-methyl-benzoic acid

: 1427274-94-9
4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]-2-methyl-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 1.5 h / 20 °C

2: ammonium hydroxide / tetrahydrofuran; water / 2 h / 20 °C

With ammonium hydroxide; oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; water;

Reference yield:

: 1427274-49-4
4-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isothiazol-3-yl]-2-methyl-benzoic acid tert-butyl ester

: 1427274-94-9
4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]-2-methyl-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 6 h / 20 °C

2: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 1.5 h / 20 °C

3: ammonium hydroxide / tetrahydrofuran; water / 2 h / 20 °C

With ammonium hydroxide; oxalyl dichloride; N,N-dimethyl-formamide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water;