4-[3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butyryl]-2-methyl-benzoic acid tert-butyl ester

Base Information

Chemical Name:4-[3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butyryl]-2-methyl-benzoic acid tert-butyl ester
CAS No.:1427274-70-1
Molecular Formula:C₂₂H₂₁Cl₂F₃O₃S
Molecular Weight:493.374
Hs Code.:

Synonyms:4-[3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butyryl]-2-methyl-benzoic acid tert-butyl ester

Suppliers and Price of 4-[3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butyryl]-2-methyl-benzoic acid tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4-[3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butyryl]-2-methyl-benzoic acid tert-butyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of 4-[3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butyryl]-2-methyl-benzoic acid tert-butyl ester

There total 1 articles about 4-[3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butyryl]-2-methyl-benzoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352242-90-0
4-[(E)-3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-but-2-enoyl]-2-methyl-benzoic acid tert-butyl ester

: 507-09-5
tiolacetic acid

: 1427274-70-1
4-[3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butyryl]-2-methyl-benzoic acid tert-butyl ester

: 1427274-67-6
4-[3-acetylsulfanyl-3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-butyryl]-2-methyl-benzoic acid tert-butyl ester

Guidance literature:: With triethylamine; at 20 ℃; for 24h;

Reference yield:

: 1427274-70-1
4-[3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butyryl]-2-methyl-benzoic acid tert-butyl ester

: 1427274-49-4
4-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isothiazol-3-yl]-2-methyl-benzoic acid tert-butyl ester

Guidance literature:: With potassium hydroxide; hydroxylamine-O-sulfonic acid; In tetrahydrofuran; water; at 20 ℃; for 0.5h;

Reference yield:

: 1427274-70-1
4-[3-(3,5-dichloro-phenyl)-4,4,4-trifluoro-3-mercapto-butyryl]-2-methyl-benzoic acid tert-butyl ester

: 1427274-51-8
4-[5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4H-isothiazol-3-yl]-2-methyl-benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine-O-sulfonic acid; potassium hydroxide / tetrahydrofuran; water / 0.5 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 6 h / 20 °C

With trifluoroacetic acid; potassium hydroxide; hydroxylamine-O-sulfonic acid; In tetrahydrofuran; dichloromethane; water;