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rac-N-{1-[(phenyl)methyl]piperidin-4-yl}-2-{2-[(2,6-diethoxyphenoxy)methyl]phenyl}-2-hydroxypropanamide

Base Information Edit
  • Chemical Name:rac-N-{1-[(phenyl)methyl]piperidin-4-yl}-2-{2-[(2,6-diethoxyphenoxy)methyl]phenyl}-2-hydroxypropanamide
  • CAS No.:1323264-19-2
  • Molecular Formula:C32H40N2O5
  • Molecular Weight:532.68
  • Hs Code.:
  • Mol file:1323264-19-2.mol
rac-N-{1-[(phenyl)methyl]piperidin-4-yl}-2-{2-[(2,6-diethoxyphenoxy)methyl]phenyl}-2-hydroxypropanamide

Synonyms:rac-N-{1-[(phenyl)methyl]piperidin-4-yl}-2-{2-[(2,6-diethoxyphenoxy)methyl]phenyl}-2-hydroxypropanamide

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Chemical Property of rac-N-{1-[(phenyl)methyl]piperidin-4-yl}-2-{2-[(2,6-diethoxyphenoxy)methyl]phenyl}-2-hydroxypropanamide Edit
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Technology Process of rac-N-{1-[(phenyl)methyl]piperidin-4-yl}-2-{2-[(2,6-diethoxyphenoxy)methyl]phenyl}-2-hydroxypropanamide

There total 6 articles about rac-N-{1-[(phenyl)methyl]piperidin-4-yl}-2-{2-[(2,6-diethoxyphenoxy)methyl]phenyl}-2-hydroxypropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
4-amino-1-benzylpiperidine; 2-{2-[(2,6-diethoxyphenoxy)methyl]phenyl}-2-hydroxypropanoic acid; With 4-methyl-morpholine; benzotriazol-1-ol; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere;
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1135/cccc2011017
Guidance literature:
Multi-step reaction with 3 steps
1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere
1.2: 0.5 h / -78 - 0 °C / Inert atmosphere
2.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 16 h
3.1: 4-methyl-morpholine; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere
3.2: 16 h / 0 - 20 °C / Inert atmosphere
With 4-methyl-morpholine; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; benzotriazol-1-ol; dimethyl sulfoxide; In dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1.2: Swern oxidation;
DOI:10.1135/cccc2011017
Guidance literature:
Multi-step reaction with 2 steps
1.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 16 h
2.1: 4-methyl-morpholine; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere
2.2: 16 h / 0 - 20 °C / Inert atmosphere
With 4-methyl-morpholine; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; benzotriazol-1-ol; In water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1135/cccc2011017
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